O-trimethylsilyl phenyl[2-(2-[4-methoxyphenyl]-1,1,1-trifluoroethyl)]hydroxylamine

Base Information

Chemical Name:O-trimethylsilyl phenyl[2-(2-[4-methoxyphenyl]-1,1,1-trifluoroethyl)]hydroxylamine
CAS No.:220880-65-9
Molecular Formula:C₁₈H₂₂F₃NO₂Si
Molecular Weight:369.459
Hs Code.:

Synonyms:O-trimethylsilyl phenyl[2-(2-[4-methoxyphenyl]-1,1,1-trifluoroethyl)]hydroxylamine

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Chemical Property of O-trimethylsilyl phenyl[2-(2-[4-methoxyphenyl]-1,1,1-trifluoroethyl)]hydroxylamine

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Technology Process of O-trimethylsilyl phenyl[2-(2-[4-methoxyphenyl]-1,1,1-trifluoroethyl)]hydroxylamine

There total 4 articles about O-trimethylsilyl phenyl[2-(2-[4-methoxyphenyl]-1,1,1-trifluoroethyl)]hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 3585-93-1
N-(4-methoxybenzylidene)aniline oxide

: 81290-20-2
(trifluoromethyl)trimethylsilane

: 220880-65-9
O-trimethylsilyl phenyl[2-(2-[4-methoxyphenyl]-1,1,1-trifluoroethyl)]hydroxylamine

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at -30 - -20 ℃; for 48h;
DOI:10.1021/jo000685l

Reference yield: 62.0%

: 3585-93-1,85225-54-3,87289-90-5
p-methoxydiphenylnitrone

: 81290-20-2
(trifluoromethyl)trimethylsilane

: 220880-65-9
O-trimethylsilyl phenyl[2-(2-[4-methoxyphenyl]-1,1,1-trifluoroethyl)]hydroxylamine

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at -20 ℃;
DOI:10.1016/S0040-4039(98)80010-5

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 220880-65-9
O-trimethylsilyl phenyl[2-(2-[4-methoxyphenyl]-1,1,1-trifluoroethyl)]hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 4 h / 20 °C

2: 90 percent / potassium t-butoxide / tetrahydrofuran / 48 h / -30 - -20 °C

With potassium tert-butylate; In tetrahydrofuran; ethanol;
DOI:10.1021/jo000685l