C₄₁H₆₇IO₇Si

Base Information

Chemical Name:C₄₁H₆₇IO₇Si
CAS No.:1207069-58-6
Molecular Formula:C₄₁H₆₇IO₇Si
Molecular Weight:826.969
Hs Code.:

C<sub>41</sub>H<sub>67</sub>IO<sub>7</sub>Si

Synonyms:C₄₁H₆₇IO₇Si

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Chemical Property of C₄₁H₆₇IO₇Si

Chemical Property:

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Technology Process of C₄₁H₆₇IO₇Si

There total 16 articles about C₄₁H₆₇IO₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: C₄₀H₆₅IO₇Si

: 1207069-58-6
C₄₁H₆₇IO₇Si

Guidance literature:: With diazomethyl-trimethyl-silane; In hexanes; benzene; at 20 ℃; for 0.75h; Inert atmosphere;
DOI:10.1021/ol902778y

Reference yield:

: 1207069-48-4
C₃₂H₄₂O₄Si

: 1207069-58-6
C₄₁H₆₇IO₇Si

Guidance literature:: Multi-step reaction with 12 steps

1: 2,6-dimethylpyridine / dichloromethane / 0 °C

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 20 °C / pH 7 / aq. buffer

3: Hoveyda-Grubbs catalyst second generation / dichloromethane / 35 °C

4: potassium tert-butylate / tetrahydrofuran / 0 °C

5: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / -60 - -25 °C

6: 10% palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C

7: Dess-Martin periodane / dichloromethane / 20 °C

8: lithium hexamethyldisilazane / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 6 h / -78 - 20 °C

9: potassium hydroxide / tetrahydrofuran; methanol / 60 °C

10: Dess-Martin periodane / dichloromethane / 20 °C

11: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 20 °C

12: methanol / benzene / 20 °C

With 2,6-dimethylpyridine; methanol; triethylsilane; sodium chlorite; sodium dihydrogenphosphate; Hoveyda-Grubbs catalyst second generation; 2-methyl-but-2-ene; 10% palladium on activated charcoal; boron trifluoride diethyl etherate; potassium tert-butylate; hydrogen; Dess-Martin periodane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; ethyl acetate; tert-butyl alcohol; benzene; 8: Julia Olefin synthesis;
DOI:10.1002/chem.201003135

Reference yield:

: 910046-59-2
tert-butyl-[(3S)-(4-methoxybenzyloxy)hex-5-enyloxy]diphenylsilane

: 1207069-58-6
C₄₁H₆₇IO₇Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water / 20 °C

1.2: 20 °C

2.1: magnesium bromide diethyl etherate / dichloromethane / 0 °C

3.1: 2,6-dimethylpyridine / dichloromethane / 0 °C

4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 20 °C / pH 7 / aq. buffer

5.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 35 °C

6.1: potassium tert-butylate / tetrahydrofuran / 0 °C

7.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / -60 - -25 °C

8.1: 10% palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C

9.1: Dess-Martin periodane / dichloromethane / 20 °C

10.1: lithium hexamethyldisilazane / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 6 h / -78 - 20 °C

11.1: potassium hydroxide / tetrahydrofuran; methanol / 60 °C

12.1: Dess-Martin periodane / dichloromethane / 20 °C

13.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 20 °C

14.1: methanol / benzene / 20 °C

With 2,6-dimethylpyridine; methanol; triethylsilane; sodium chlorite; sodium dihydrogenphosphate; osmium(VIII) oxide; Hoveyda-Grubbs catalyst second generation; magnesium bromide diethyl etherate; 2-methyl-but-2-ene; 10% palladium on activated charcoal; boron trifluoride diethyl etherate; potassium tert-butylate; hydrogen; Dess-Martin periodane; 4-methylmorpholine N-oxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; ethyl acetate; tert-butyl alcohol; benzene; 10.1: Julia Olefin synthesis;
DOI:10.1002/chem.201003135