(1E,3E)-4-Phenyl-buta-1,3-diene-1-sulfonic acid allyl-(4-chloro-benzyl)-amide

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Chemical Name:(1E,3E)-4-Phenyl-buta-1,3-diene-1-sulfonic acid allyl-(4-chloro-benzyl)-amide
CAS No.:329010-38-0
Molecular Formula:C₂₀H₂₀ClNO₂S
Molecular Weight:373.903
Hs Code.:

Synonyms:(1E,3E)-4-Phenyl-buta-1,3-diene-1-sulfonic acid allyl-(4-chloro-benzyl)-amide

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Chemical Property of (1E,3E)-4-Phenyl-buta-1,3-diene-1-sulfonic acid allyl-(4-chloro-benzyl)-amide

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Technology Process of (1E,3E)-4-Phenyl-buta-1,3-diene-1-sulfonic acid allyl-(4-chloro-benzyl)-amide

There total 3 articles about (1E,3E)-4-Phenyl-buta-1,3-diene-1-sulfonic acid allyl-(4-chloro-benzyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 106-95-6
allyl bromide

: 204857-48-7
(1E,3E)-4-Phenyl-buta-1,3-diene-1-sulfonic acid 4-chloro-benzylamide

: 329010-38-0
(1E,3E)-4-Phenyl-buta-1,3-diene-1-sulfonic acid allyl-(4-chloro-benzyl)-amide

Guidance literature:: (1E,3E)-4-Phenyl-buta-1,3-diene-1-sulfonic acid 4-chloro-benzylamide; With sodium hydride; In tetrahydrofuran;

allyl bromide; In tetrahydrofuran; Further stages.; Heating;
DOI:10.1021/ol006863e

Reference yield:

: 104-55-2
3-phenyl-propenal

: 329010-38-0
(1E,3E)-4-Phenyl-buta-1,3-diene-1-sulfonic acid allyl-(4-chloro-benzyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: t-BuOK / tetrahydrofuran / 1 h / -78 °C

1.2: 99 percent / tetrahydrofuran / 18 h / -78 - 20 °C

2.1: NaH / tetrahydrofuran

2.2: 82 percent / tetrahydrofuran / Heating

With potassium tert-butylate; sodium hydride; In tetrahydrofuran;
DOI:10.1021/ol006863e

Reference yield:

: 204857-35-2
N-(tert-butoxycarbonyl)-N-(4-chlorobenzyl)-methanesulfonamide

: 329010-38-0
(1E,3E)-4-Phenyl-buta-1,3-diene-1-sulfonic acid allyl-(4-chloro-benzyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: t-BuOK / tetrahydrofuran / 1 h / -78 °C

1.2: 99 percent / tetrahydrofuran / 18 h / -78 - 20 °C

2.1: NaH / tetrahydrofuran

2.2: 82 percent / tetrahydrofuran / Heating

With potassium tert-butylate; sodium hydride; In tetrahydrofuran;
DOI:10.1021/ol006863e