2,5-diphenyl-[1,4,2,5]dioxadiarsinane

Base Information

• Chemical Name: 2,5-diphenyl-[1,4,2,5]dioxadiarsinane
• CAS No.: 861318-69-6
• Molecular Formula: C₁₄H₁₄As₂O₂
• Molecular Weight: 364.107
• Mol file: 861318-69-6.mol

Synonyms:2,5-diphenyl-[1,4,2,5]dioxadiarsinane

Chemical Property of 2,5-diphenyl-[1,4,2,5]dioxadiarsinane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,5-diphenyl-[1,4,2,5]dioxadiarsinane

There total 3 articles about 2,5-diphenyl-[1,4,2,5]dioxadiarsinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylarsonic acid (98-05-5) → 2,5-diphenyl-[1,4,2,5]dioxadiarsinane (861318-69-6)

Guidance literature:

Multi-step reaction with 2 steps

1: amalgamated zinc; concentrated hydrochloric acid; diethyl ether

2: concentrated hydrochloric acid

With hydrogenchloride; amalgamated zinc; diethyl ether;

Reference yield:

benzene diazonium chloride (100-34-5) → 2,5-diphenyl-[1,4,2,5]dioxadiarsinane (861318-69-6)

Guidance literature:

Multi-step reaction with 3 steps

1: water; copper sulfate; sodium arsenite / 15 °C

2: amalgamated zinc; concentrated hydrochloric acid; diethyl ether

3: concentrated hydrochloric acid

With hydrogenchloride; copper(I) sulfate; trisodium arsenite; amalgamated zinc; diethyl ether; water; copper(II) sulfate;

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + phenylarsane (822-65-1) → 2,5-diphenyl-[1,4,2,5]dioxadiarsinane (861318-69-6)

Guidance literature:

With hydrogenchloride;

upstream raw materials:

formaldehyd

phenylarsane

phenylarsonic acid

benzene diazonium chloride

Downstream raw materials:

phenylarsine oxide