methyl 2-bromononanoate

Base Information

• Chemical Name: methyl 2-bromononanoate
• CAS No.: 26040-75-5
• Molecular Formula: C₁₀H₁₉BrO₂
• Molecular Weight: 251.164
• Mol file: 26040-75-5.mol

Synonyms:methyl 2-bromononanoate

Chemical Property of methyl 2-bromononanoate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of methyl 2-bromononanoate

There total 1 articles about methyl 2-bromononanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

methanol (67-56-1) + nonan-1-al (124-19-6) → nonanoic acid methyl ester (1731-84-6) + methyl 2-bromononanoate (26040-75-5)

Guidance literature:

nonan-1-al; With ammonium cerium (IV) nitrate; lithium bromide; In neat liquid;

methanol; In neat liquid; at 35 - 40 ℃; for 3.5h;

DOI:10.1016/j.tetlet.2016.12.036

Reference yield: 70.0%

2-(4-methoxyphenoxy)pyridine (78646-39-6) + methyl 2-bromononanoate (26040-75-5) → methyl 2-(2-methoxy-5-(pyridin-2-yloxy)phenyl)octanoate

Guidance literature:

With [RhCl₂(p-cymene)]2; potassium carbonate; (adamant-1-yl)-acetic acid; In benzene; at 120 ℃; for 24h; Sealed tube; Inert atmosphere;

DOI:10.1021/acs.orglett.7b00885

Reference yield:

methyl 2-bromononanoate (26040-75-5) → 2-[(2,4-Dinitro-phenyl)-hydrazono]-nonanoic acid methyl ester

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaNO₂ / ethanol

With sodium nitrite; In ethanol;

DOI:10.1007/BF00908991

upstream raw materials:

methanol

nonan-1-al

Downstream raw materials:

methyl (2E)-2-nonenoate