N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-N'-(tert-butyloxycarbonyl)-D-lysine methyl ester

Base Information

Chemical Name:N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-N'-(tert-butyloxycarbonyl)-D-lysine methyl ester
CAS No.:110473-30-8
Molecular Formula:C₃₁H₃₆Cl₅N₃O₉
Molecular Weight:771.907
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-N'-(tert-butyloxycarbonyl)-D-lysine methyl ester

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Chemical Property of N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-N'-(tert-butyloxycarbonyl)-D-lysine methyl ester

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Technology Process of N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-N'-(tert-butyloxycarbonyl)-D-lysine methyl ester

There total 6 articles about N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-N'-(tert-butyloxycarbonyl)-D-lysine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 87-86-5,67471-28-7
Pentachlorophenol

: 110473-28-4
N-(benzyloxycarbonyl)-D-glutamyl-N'-(tert-butyloxycarbonyl)-D-lysine methyl ester

: 110473-30-8
N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-N'-(tert-butyloxycarbonyl)-D-lysine methyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; for 22h;
DOI:10.1021/jo00233a006

Reference yield:

: 66845-42-9
N^α-(benzyloxycarbonyl)-N^ε-(tert-butoxycarbonyl)-D-lysine

: 110473-30-8
N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-N'-(tert-butyloxycarbonyl)-D-lysine methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / ethanol; diethyl ether / 0.5 h / 0 °C

2: 100 percent / H₂ / 10percent Pd/C / methanol / 4 h / 760 Torr

3: 42 percent / tetrahydrofuran / 22 h

4: 91 percent / N,N'-dicyclohexylcarbodiimide (DCC) / tetrahydrofuran; CH₂Cl₂ / 22 h

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jo00233a006

Reference yield:

: 84559-78-4
methyl (2R)-2-[[(benzyloxy)carbonyl]amino]-6-[[(tert-butoxy)carbonyl]amino]hexanoate

: 110473-30-8
N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-N'-(tert-butyloxycarbonyl)-D-lysine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / H₂ / 10percent Pd/C / methanol / 4 h / 760 Torr

2: 42 percent / tetrahydrofuran / 22 h

3: 91 percent / N,N'-dicyclohexylcarbodiimide (DCC) / tetrahydrofuran; CH₂Cl₂ / 22 h

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo00233a006