N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-D-lysine methyl ester, hydrochloride salt

Base Information

Chemical Name:N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-D-lysine methyl ester, hydrochloride salt
CAS No.:110473-32-0
Molecular Formula:C₂₆H₂₈Cl₅N₃O₇*ClH
Molecular Weight:708.25
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-D-lysine methyl ester, hydrochloride salt

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Chemical Property of N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-D-lysine methyl ester, hydrochloride salt

Chemical Property:

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Technology Process of N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-D-lysine methyl ester, hydrochloride salt

There total 7 articles about N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-D-lysine methyl ester, hydrochloride salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 110473-30-8
N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-N'-(tert-butyloxycarbonyl)-D-lysine methyl ester

: 110473-32-0
N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-D-lysine methyl ester, hydrochloride salt

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; for 4h;
DOI:10.1021/jo00233a006

Reference yield:

: 66845-42-9
N^α-(benzyloxycarbonyl)-N^ε-(tert-butoxycarbonyl)-D-lysine

: 110473-32-0
N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-D-lysine methyl ester, hydrochloride salt

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / ethanol; diethyl ether / 0.5 h / 0 °C

2: 100 percent / H₂ / 10percent Pd/C / methanol / 4 h / 760 Torr

3: 42 percent / tetrahydrofuran / 22 h

4: 91 percent / N,N'-dicyclohexylcarbodiimide (DCC) / tetrahydrofuran; CH₂Cl₂ / 22 h

5: 100 percent / HCl / dioxane / 4 h

With hydrogenchloride; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jo00233a006

Reference yield:

: 84559-78-4
methyl (2R)-2-[[(benzyloxy)carbonyl]amino]-6-[[(tert-butoxy)carbonyl]amino]hexanoate

: 110473-32-0
N-(benzyloxycarbonyl)-γ-(pentachlorophenyl)-D-glutamyl-D-lysine methyl ester, hydrochloride salt

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / H₂ / 10percent Pd/C / methanol / 4 h / 760 Torr

2: 42 percent / tetrahydrofuran / 22 h

3: 91 percent / N,N'-dicyclohexylcarbodiimide (DCC) / tetrahydrofuran; CH₂Cl₂ / 22 h

4: 100 percent / HCl / dioxane / 4 h

With hydrogenchloride; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;
DOI:10.1021/jo00233a006