C₂HF₃O₂*C₃₂H₄₀N₄O₃

Base Information

Chemical Name:C₂HF₃O₂*C₃₂H₄₀N₄O₃
CAS No.:373637-03-7
Molecular Formula:C₂HF₃O₂*C₃₂H₄₀N₄O₃
Molecular Weight:642.719
Hs Code.:

C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>*C<sub>32</sub>H<sub>40</sub>N<sub>4</sub>O<sub>3</sub>

Synonyms:C₂HF₃O₂*C₃₂H₄₀N₄O₃

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Chemical Property of C₂HF₃O₂*C₃₂H₄₀N₄O₃

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Technology Process of C₂HF₃O₂*C₃₂H₄₀N₄O₃

There total 6 articles about C₂HF₃O₂*C₃₂H₄₀N₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 103-71-9
phenyl isocyanate

: 76-05-1
trifluoroacetic acid

: 373638-29-0
6-benzyloxy-1,2,3,4-tetrahydro-isoquinoline-1-carboxylic acid (2-diisopropylamino-ethyl)-amide

: 373637-03-7
C₂HF₃O₂*C₃₂H₄₀N₄O₃

Guidance literature:: phenyl isocyanate; 6-benzyloxy-1,2,3,4-tetrahydro-isoquinoline-1-carboxylic acid (2-diisopropylamino-ethyl)-amide; In dichloromethane;

trifluoroacetic acid; In methanol; water;

Reference yield:

: 2039-67-0
2-(3-methoxyphenyl)-1-ethanamine

: 373637-03-7
C₂HF₃O₂*C₃₂H₄₀N₄O₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: water; hydrogen bromide / 18 h / 4 - 140 °C / Heating / reflux

2.1: ethanol / 2 h / 4 - 20 °C

3.1: hydrogenchloride / 48 h / Heating / reflux

4.1: triethylamine / tetrahydrofuran / 18 h / 20 °C

5.1: sodium methylate / methanol / 2 h / 20 - 22 °C

5.2: 22 - 34 °C

6.1: potassium carbonate / DMF (N,N-dimethyl-formamide)

7.1: sodium hydroxide; water / tetrahydrofuran; methanol / 2.67 h / 23 - 40 °C

8.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / DMF (N,N-dimethyl-formamide) / 20 °C

9.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

9.2: pH ~ 8

10.1: dichloromethane

With hydrogenchloride; sodium hydroxide; 1-hydroxy-7-aza-benzotriazole; water; hydrogen bromide; sodium methylate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane;

Reference yield:

: 588-05-6
m-tyramine

: 373637-03-7
C₂HF₃O₂*C₃₂H₄₀N₄O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: ethanol / 2 h / 4 - 20 °C

2.1: hydrogenchloride / 48 h / Heating / reflux

3.1: triethylamine / tetrahydrofuran / 2 h / 20 °C

4.1: potassium carbonate / DMF (N,N-dimethyl-formamide)

5.1: sodium hydroxide; water / tetrahydrofuran; methanol / 2.67 h / 23 - 40 °C

6.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / DMF (N,N-dimethyl-formamide) / 20 °C

7.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

7.2: pH ~ 8

8.1: dichloromethane

With hydrogenchloride; sodium hydroxide; 1-hydroxy-7-aza-benzotriazole; water; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane;