Technology Process of 9-benzenesulfonyl-3-methoxycarbazole
There total 4 articles about 9-benzenesulfonyl-3-methoxycarbazole which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
[iridium bis(2-(2,4-difluorophenyl)pyridinate) (9,10-phenanthroline)]hexafluorophosphate; oxygen; palladium diacetate;
In
dimethyl sulfoxide;
at 80 ℃;
Sealed tube;
Irradiation;
DOI:10.1021/acscatal.5b00817
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine / dichloromethane / 16 h / 20 °C / Inert atmosphere
2: [bis(acetoxy)iodo]benzene; copper(II) bis(trifluoromethanesulfonate); trifluoroacetic acid / 1,2-dichloro-ethane / 0.25 h / 50 °C
With
pyridine; [bis(acetoxy)iodo]benzene; copper(II) bis(trifluoromethanesulfonate); trifluoroacetic acid;
In
dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ja111652v
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water; toluene / 16 h / 100 °C
2: pyridine / dichloromethane / 16 h / 20 °C / Inert atmosphere
3: [bis(acetoxy)iodo]benzene; copper(II) bis(trifluoromethanesulfonate); trifluoroacetic acid / 1,2-dichloro-ethane / 0.25 h / 50 °C
With
pyridine; tetrakis(triphenylphosphine) palladium(0); [bis(acetoxy)iodo]benzene; copper(II) bis(trifluoromethanesulfonate); potassium carbonate; trifluoroacetic acid;
In
ethanol; dichloromethane; water; 1,2-dichloro-ethane; toluene;
1: Suzuki-Miyaura coupling;
DOI:10.1021/ja111652v
