N,N''-[(benzyl)-N,N',N''-[(6-methoxycarbonyl)pyridine-2-yl]methyl]diethylenetriamine

Base Information

Chemical Name:N,N''-[(benzyl)-N,N',N''-[(6-methoxycarbonyl)pyridine-2-yl]methyl]diethylenetriamine
CAS No.:1332368-11-2
Molecular Formula:C₄₂H₄₆N₆O₆
Molecular Weight:730.864
Hs Code.:

Synonyms:N,N''-[(benzyl)-N,N',N''-[(6-methoxycarbonyl)pyridine-2-yl]methyl]diethylenetriamine

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Chemical Property of N,N''-[(benzyl)-N,N',N''-[(6-methoxycarbonyl)pyridine-2-yl]methyl]diethylenetriamine

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Technology Process of N,N''-[(benzyl)-N,N',N''-[(6-methoxycarbonyl)pyridine-2-yl]methyl]diethylenetriamine

There total 3 articles about N,N''-[(benzyl)-N,N',N''-[(6-methoxycarbonyl)pyridine-2-yl]methyl]diethylenetriamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 17327-80-9
N¹-benzyl-N²-(2-(benzylamino)ethyl)ethane-1,2-diamine

: 146462-25-1
methyl 6-(bromomethyl)picolinate

: 1332368-11-2
N,N''-[(benzyl)-N,N',N''-[(6-methoxycarbonyl)pyridine-2-yl]methyl]diethylenetriamine

Guidance literature:: With sodium carbonate; In acetonitrile; at 60 ℃; for 20h; Inert atmosphere;
DOI:10.1139/cjc-2013-0542

Reference yield:

: 19093-67-5
(7E)-N**⁽¹⁾-benzylidene-N**⁽²⁾[(E)-2-(benzylideneamino)ethyl]ethane-1,2-diamine

: 1332368-11-2
N,N''-[(benzyl)-N,N',N''-[(6-methoxycarbonyl)pyridine-2-yl]methyl]diethylenetriamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; methanol / 2.5 h / 0 °C

2: sodium carbonate / acetonitrile / Reflux; Inert atmosphere

With methanol; sodium tetrahydroborate; sodium carbonate; In acetonitrile;

Reference yield:

: 100-52-7
benzaldehyde

: 1332368-11-2
N,N''-[(benzyl)-N,N',N''-[(6-methoxycarbonyl)pyridine-2-yl]methyl]diethylenetriamine

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / Reflux

2: sodium tetrahydroborate; methanol / 2.5 h / 0 °C

3: sodium carbonate / acetonitrile / Reflux; Inert atmosphere

With methanol; sodium tetrahydroborate; sodium carbonate; In methanol; acetonitrile;