2-(4-Ethoxy-phenyl)-acrylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Base Information

Chemical Name:2-(4-Ethoxy-phenyl)-acrylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester
CAS No.:192710-53-5
Molecular Formula:C₂₇H₃₄O₃
Molecular Weight:406.565
Hs Code.:

Synonyms:2-(4-Ethoxy-phenyl)-acrylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

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Chemical Property of 2-(4-Ethoxy-phenyl)-acrylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

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Technology Process of 2-(4-Ethoxy-phenyl)-acrylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

There total 3 articles about 2-(4-Ethoxy-phenyl)-acrylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 192710-50-2
(4-Ethoxy-phenyl)-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

: 192710-53-5
2-(4-Ethoxy-phenyl)-acrylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Guidance literature:: With potassium carbonate; N-benzyl-N,N,N-triethylammonium chloride; In cyclohexane; at 80 ℃; for 8h;
DOI:10.1016/S0040-4039(97)00878-2

Reference yield:

: 65253-04-5
(-)-8-phenylmenthol

: 192710-53-5
2-(4-Ethoxy-phenyl)-acrylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / triethylamine / CH₂Cl₂

2: 91 percent / K₂CO₃ / triethylbenzylammonium chloride / cyclohexane / 8 h / 80 °C

With potassium carbonate; triethylamine; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; cyclohexane;
DOI:10.1016/S0040-4039(97)00878-2

Reference yield:

: 10368-35-1
4-ethoxyphenylacetic acid chloride

: 192710-53-5
2-(4-Ethoxy-phenyl)-acrylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / triethylamine / CH₂Cl₂

2: 91 percent / K₂CO₃ / triethylbenzylammonium chloride / cyclohexane / 8 h / 80 °C

With potassium carbonate; triethylamine; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; cyclohexane;
DOI:10.1016/S0040-4039(97)00878-2