pent-4-enyl 3-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

Base Information

Chemical Name:pent-4-enyl 3-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside
CAS No.:189218-61-9
Molecular Formula:C₃₀H₃₇NO₇
Molecular Weight:523.626
Hs Code.:

Synonyms:pent-4-enyl 3-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

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Chemical Property of pent-4-enyl 3-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

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Technology Process of pent-4-enyl 3-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

There total 4 articles about pent-4-enyl 3-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 189218-60-8
pent-4-enyl 3,6-di-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

: 189218-61-9
pent-4-enyl 3-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; dichloromethane; at 0 ℃; for 7h;
DOI:10.1021/jo961668s

Reference yield:

: 100-39-0
benzyl bromide

: 189218-61-9
pent-4-enyl 3-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / Bu₄NI, NaH / dimethylformamide / 0.33 h / Ambient temperature

2: 75 percent / NaOMe / CH₂Cl₂; methanol / 7 h / 0 °C

With sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo961668s

Reference yield:

: 163926-96-3
Pent-4-enyl 3,4,6-tri-O-acetyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

: 189218-61-9
pent-4-enyl 3-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: NaOMe / CH₂Cl₂; methanol / 1 h / Ambient temperature

2: pyridine / 2 h / -40 °C

3: 80 percent / Bu₄NI, NaH / dimethylformamide / 0.33 h / Ambient temperature

4: 75 percent / NaOMe / CH₂Cl₂; methanol / 7 h / 0 °C

With pyridine; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo961668s