pent-4-enyl 3,6-di-O-benzoyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

Base Information

Chemical Name:pent-4-enyl 3,6-di-O-benzoyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside
CAS No.:189218-59-5
Molecular Formula:C₃₀H₃₅NO₈
Molecular Weight:537.61
Hs Code.:

Synonyms:pent-4-enyl 3,6-di-O-benzoyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pent-4-enyl 3,6-di-O-benzoyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

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Technology Process of pent-4-enyl 3,6-di-O-benzoyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

There total 2 articles about pent-4-enyl 3,6-di-O-benzoyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 163926-96-3
Pent-4-enyl 3,4,6-tri-O-acetyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

: 189218-59-5
pent-4-enyl 3,6-di-O-benzoyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: NaOMe / CH₂Cl₂; methanol / 1 h / Ambient temperature

2: pyridine / 2 h / -40 °C

With pyridine; sodium methylate; In methanol; dichloromethane;
DOI:10.1021/jo961668s

Reference yield:

: 98-88-4
benzoyl chloride

: Pent-4-enoic acid ((2R,3R,4R,5S,6R)-4,5-dihydroxy-6-hydroxymethyl-2-pent-4-enyloxy-tetrahydro-pyran-3-yl)-amide

: 189218-59-5
pent-4-enyl 3,6-di-O-benzoyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

Guidance literature:: With pyridine; at -40 ℃; for 2h; Yield given;
DOI:10.1021/jo961668s

Reference yield: 80.0%

: 100-39-0
benzyl bromide

: 189218-59-5
pent-4-enyl 3,6-di-O-benzoyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

: 189218-60-8
pent-4-enyl 3,6-di-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; for 0.333333h; Ambient temperature;
DOI:10.1021/jo961668s