pent-4-enyl 3,6-di-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

Base Information

Chemical Name:pent-4-enyl 3,6-di-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside
CAS No.:189218-60-8
Molecular Formula:C₃₇H₄₁NO₈
Molecular Weight:627.734
Hs Code.:

Synonyms:pent-4-enyl 3,6-di-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

Suppliers and Price of pent-4-enyl 3,6-di-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of pent-4-enyl 3,6-di-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of pent-4-enyl 3,6-di-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

There total 3 articles about pent-4-enyl 3,6-di-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 100-39-0
benzyl bromide

: 189218-59-5
pent-4-enyl 3,6-di-O-benzoyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

: 189218-60-8
pent-4-enyl 3,6-di-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; for 0.333333h; Ambient temperature;
DOI:10.1021/jo961668s

Reference yield:

: 98-88-4
benzoyl chloride

: 189218-60-8
pent-4-enyl 3,6-di-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 2 h / -40 °C

2: 80 percent / Bu₄NI, NaH / dimethylformamide / 0.33 h / Ambient temperature

With pyridine; tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jo961668s

Reference yield:

: 163926-96-3
Pent-4-enyl 3,4,6-tri-O-acetyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

: 189218-60-8
pent-4-enyl 3,6-di-O-benzoyl-4-O-benzyl-2-deoxy-2-(pent-4-enoylamino)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: NaOMe / CH₂Cl₂; methanol / 1 h / Ambient temperature

2: pyridine / 2 h / -40 °C

3: 80 percent / Bu₄NI, NaH / dimethylformamide / 0.33 h / Ambient temperature

With pyridine; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo961668s