3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-benzyloxycarbonylaminopropionic acid methyl ester

Base Information

Chemical Name:3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-benzyloxycarbonylaminopropionic acid methyl ester
CAS No.:939378-04-8
Molecular Formula:C₃₆H₄₉N₂O₈P
Molecular Weight:668.767
Hs Code.:

3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-benzyloxycarbonylaminopropionic acid methyl ester

Synonyms:3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-benzyloxycarbonylaminopropionic acid methyl ester

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Chemical Property of 3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-benzyloxycarbonylaminopropionic acid methyl ester

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Technology Process of 3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-benzyloxycarbonylaminopropionic acid methyl ester

There total 3 articles about 3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-benzyloxycarbonylaminopropionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 768-90-1
1-Adamantyl bromide

: 939378-02-6
2-benzyloxycarbonylamino-3-[(1-tert-butyloxycarbonylamino-3-phenylpropyl)hydroxyphosphinoyl]propionic acid methyl ester

: 939378-04-8
3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-benzyloxycarbonylaminopropionic acid methyl ester

Guidance literature:: With silver(l) oxide; In chloroform; Heating;
DOI:10.1016/j.bmc.2007.02.042

Reference yield:

: 21149-17-7
methyl 2-(benzyloxycarbonylamino)acrylate

: 939378-04-8
3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-benzyloxycarbonylaminopropionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / hexamethyldisilazane / Heating

2: 80 percent / silver oxide / CHCl₃ / Heating

With 1,1,1,3,3,3-hexamethyl-disilazane; silver(l) oxide; In chloroform;
DOI:10.1016/j.bmc.2007.02.042

Reference yield:

: 260390-87-2
(1-(N-(tert-butyloxycarbonyl)amino)-3-phenylpropyl) phosphinic acid

: 939378-04-8
3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-benzyloxycarbonylaminopropionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / hexamethyldisilazane / Heating

2: 80 percent / silver oxide / CHCl₃ / Heating

With 1,1,1,3,3,3-hexamethyl-disilazane; silver(l) oxide; In chloroform;
DOI:10.1016/j.bmc.2007.02.042