3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-aminopropionic acid methyl ester

Base Information

Chemical Name:3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-aminopropionic acid methyl ester
CAS No.:939377-99-8
Molecular Formula:C₂₈H₄₃N₂O₆P
Molecular Weight:534.633
Hs Code.:

Synonyms:3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-aminopropionic acid methyl ester

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Chemical Property of 3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-aminopropionic acid methyl ester

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Technology Process of 3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-aminopropionic acid methyl ester

There total 3 articles about 3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-aminopropionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 939378-04-8
3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-benzyloxycarbonylaminopropionic acid methyl ester

: 939377-99-8
3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-aminopropionic acid methyl ester

Guidance literature:: With hydrogen; Pd-BaSO₄; In methanol; water; for 3.5h;
DOI:10.1016/j.bmc.2007.02.042

Reference yield:

: 939378-02-6
2-benzyloxycarbonylamino-3-[(1-tert-butyloxycarbonylamino-3-phenylpropyl)hydroxyphosphinoyl]propionic acid methyl ester

: 939377-99-8
3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-aminopropionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / silver oxide / CHCl₃ / Heating

2: 100 percent / H₂ / Pd/BaSO₄ / methanol; H₂O / 3.5 h

With hydrogen; silver(l) oxide; Pd-BaSO₄; In methanol; chloroform; water;
DOI:10.1016/j.bmc.2007.02.042

Reference yield:

: 260390-87-2
(1-(N-(tert-butyloxycarbonyl)amino)-3-phenylpropyl) phosphinic acid

: 939377-99-8
3-[(adamantan-1-yloxy)-(1-tert-butyloxycarbonylamino-3-phenylpropyl)phosphinoyl]-2-aminopropionic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / hexamethyldisilazane / Heating

2: 80 percent / silver oxide / CHCl₃ / Heating

3: 100 percent / H₂ / Pd/BaSO₄ / methanol; H₂O / 3.5 h

With hydrogen; 1,1,1,3,3,3-hexamethyl-disilazane; silver(l) oxide; Pd-BaSO₄; In methanol; chloroform; water;
DOI:10.1016/j.bmc.2007.02.042