FMOC-MET-OSU

Base Information

• Chemical Name: FMOC-MET-OSU
• CAS No.: 112913-64-1
• Molecular Formula: C24H24 N2 O6 S
• Molecular Weight: 468.52
• Mol file: 112913-64-1.mol

Synonyms:Carbamicacid, [1-[[(2,5-dioxo-1-pyrrolidinyl)oxy]carbonyl]-3-(methylthio)propyl]-,9H-fluoren-9-ylmethyl ester, (S)- (9CI)

Chemical Property of FMOC-MET-OSU

Chemical Property:

• PKA: 9.94±0.46(Predicted)
• PSA: 127.31000
• Density: 1.39±0.1 g/cm3(Predicted)
• LogP: 3.58280
• Storage Temp.: Store at 0°C

Purity/Quality:

97% ^*data from raw suppliers

Fmoc-L-methionine N-hydroxysuccinimide ester ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of FMOC-MET-OSU

There total 1 articles about FMOC-MET-OSU which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-hydroxy-pyrrolidine-2,5-dione (6066-82-6) + N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-methionine (71989-28-1) → Fmoc-Met-OSu (112913-64-1)

Guidance literature:

With dicyclohexyl-carbodiimide; In tetrahydrofuran; at 0 ℃; for 2.5h;

DOI:10.1002/1521-3765(20010316)7:6<1184::AID-CHEM1184>3.0.CO;2-5

Reference yield: 92.0%

4-nitrophenyl azide (1516-60-5) + Fmoc-Met-OSu (112913-64-1) → Nα-(9-fluorenyloxycarbonyl)-L-methionyl-p-nitroanilide

Guidance literature:

Fmoc-Met-OSu; With sodium hydrogen selenide; In tetrahydrofuran; isopropyl alcohol; at 0 - 5 ℃; for 1h; Inert atmosphere;

4-nitrophenyl azide; In tetrahydrofuran; isopropyl alcohol; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.3762/bjoc.7.117

Reference yield:

L-Asp(t-Bu) (3057-74-7) + N-cyclohexyl-cyclohexanamine (101-83-7) + Fmoc-Met-OSu (112913-64-1) → Fmoc-Met-Asp(OtBu)-OH dicyclohexylamine salt

Guidance literature:

L-Asp(t-Bu); Fmoc-Met-OSu; With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃;

N-cyclohexyl-cyclohexanamine; In ethyl acetate;

upstream raw materials:

1-hydroxy-pyrrolidine-2,5-dione

N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-methionine

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