N-[(1S,2R)-2-hydroxy-2-(3-methoxyphenyl)-1-methyl-ethyl]-4-nitro-benzene sulfonamide

Base Information

Chemical Name:N-[(1S,2R)-2-hydroxy-2-(3-methoxyphenyl)-1-methyl-ethyl]-4-nitro-benzene sulfonamide
CAS No.:1417334-60-1
Molecular Formula:C₁₆H₁₈N₂O₆S
Molecular Weight:366.395
Hs Code.:

Synonyms:N-[(1S,2R)-2-hydroxy-2-(3-methoxyphenyl)-1-methyl-ethyl]-4-nitro-benzene sulfonamide

Suppliers and Price of N-[(1S,2R)-2-hydroxy-2-(3-methoxyphenyl)-1-methyl-ethyl]-4-nitro-benzene sulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(1S,2R)-2-hydroxy-2-(3-methoxyphenyl)-1-methyl-ethyl]-4-nitro-benzene sulfonamide

Chemical Property:

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Technology Process of N-[(1S,2R)-2-hydroxy-2-(3-methoxyphenyl)-1-methyl-ethyl]-4-nitro-benzene sulfonamide

There total 1 articles about N-[(1S,2R)-2-hydroxy-2-(3-methoxyphenyl)-1-methyl-ethyl]-4-nitro-benzene sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1034156-00-7
(1R,2S)-2-amino-1-(3-methoxyphenyl)propan-1-ol hydrochloride

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 1417334-60-1
N-[(1S,2R)-2-hydroxy-2-(3-methoxyphenyl)-1-methyl-ethyl]-4-nitro-benzene sulfonamide

Guidance literature:: With 4-methyl-morpholine; In 2-methyltetrahydrofuran; at 40 ℃; for 1.5h; Industrial scale;

Reference yield:

: 1417334-60-1
N-[(1S,2R)-2-hydroxy-2-(3-methoxyphenyl)-1-methyl-ethyl]-4-nitro-benzene sulfonamide

: 124-63-0
methanesulfonyl chloride

: 1417334-61-2
[(1R,2S)-1-(3-methoxyphenyl)-2-[(4-nitrophenyl)sulfonylamino]propyl] methanesulfonate

Guidance literature:: In 2-methyltetrahydrofuran; at 40 ℃; for 16.16h; Industrial scale;

Reference yield:

: 1417334-60-1
N-[(1S,2R)-2-hydroxy-2-(3-methoxyphenyl)-1-methyl-ethyl]-4-nitro-benzene sulfonamide

: 1417334-62-3
(2S,3S)-2-(3-methoxyphenyl)-3-methyl-1-(4-nitrophenyl)sulfonyl-aziridine

Guidance literature:: Multi-step reaction with 2 steps

1: 2-methyltetrahydrofuran / 16.16 h / 40 °C / Industrial scale

2: hydrogenchloride / water / Industrial scale

With hydrogenchloride; In 2-methyltetrahydrofuran; water;