(2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid butyl ester

Base Information

Chemical Name:(2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid butyl ester
CAS No.:1442452-21-2
Molecular Formula:C₁₉H₁₉F₅NO₅P
Molecular Weight:467.329
Hs Code.:

Synonyms:(2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid butyl ester

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Chemical Property of (2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid butyl ester

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Technology Process of (2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid butyl ester

There total 10 articles about (2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 770-12-7
O-phenyl phosphorodichloridate

: 174468-17-8
(S)-alanine n-butyl ester hydrochloride

: 1442452-21-2
(2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid butyl ester

Guidance literature:: O-phenyl phosphorodichloridate; (S)-alanine n-butyl ester hydrochloride; With triethylamine; In dichloromethane; at -78 - 0 ℃; for 4.5h;

2,3,4,5,6-pentafluorophenol; With triethylamine; In dichloromethane; at 0 ℃; for 4.33h;
DOI:10.1021/acsmedchemlett.6b00270

Reference yield: 5.8%

: 2885-02-1,44924-99-4,50833-19-7
(S)-butyl 2-aminopropanoate

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 770-12-7
O-phenyl phosphorodichloridate

: 1442452-21-2
(2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid butyl ester

Guidance literature:: (S)-butyl 2-aminopropanoate; O-phenyl phosphorodichloridate; With triethylamine; In dichloromethane; at -20 - 0 ℃; for 1.91667h;

2,3,4,5,6-pentafluorophenol; In dichloromethane; at 20 ℃;

Reference yield: 5.8%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 73072-94-3
(S)-butyl 2-aminopropanoate tosylate salt

: 770-12-7
O-phenyl phosphorodichloridate

: 1442452-21-2
(2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid butyl ester

Guidance literature:: (S)-butyl 2-aminopropanoate tosylate salt; O-phenyl phosphorodichloridate; With triethylamine; In dichloromethane; at -20 - 0 ℃; for 1.91667h;

2,3,4,5,6-pentafluorophenol; With triethylamine; In dichloromethane; at 0 - 20 ℃;