2-propylethoxybenzene

Base Information

• Chemical Name: 2-propylethoxybenzene
• CAS No.: 101144-90-5
• Molecular Formula: C₁₁H₁₆O
• Molecular Weight: 164.247
• Mol file: 101144-90-5.mol

Synonyms:2-propylethoxybenzene

Chemical Property of 2-propylethoxybenzene

Chemical Property:

• Refractive Index: 1.4940
• Boiling Point: 213°C (estimate)
• Density: 0.9240

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-propylethoxybenzene

There total 8 articles about 2-propylethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

→ 2-propylethoxybenzene (101144-90-5)

Guidance literature:

Reference yield: 30.0%

2-(2-bromo-2-propen-1-yl)cyclohexanone (53626-84-9) + orthoformic acid triethyl ester (122-51-0) → 2-propylethoxybenzene (101144-90-5)

Guidance literature:

2-(2-bromo-2-propen-1-yl)cyclohexanone; orthoformic acid triethyl ester; With acetyl chloride; In ethanol;

With potassium tert-butylate; In dimethyl sulfoxide; at 80 ℃; for 3h; Inert atmosphere;

DOI:10.1002/hlca.200890124

Reference yield:

diethyl sulfate (64-67-5) + 2-methylmethoxybenzene (578-58-5) → 2-ethoxy-1-ethybenzene (29643-62-7) + o-propylanisole (13629-73-7) + 2-propylethoxybenzene (101144-90-5) + o-s-butylanisole (18272-71-4,96346-16-6)

Guidance literature:

With n-butyllithium; hexane; potassium tert-butylate; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given; 1) heptane, room temperature, 2 h, 2) THF;

DOI:10.1021/jo00291a044

upstream raw materials:

diethyl sulfate

2-methylmethoxybenzene

ethanol

1-(2-Propenyl)-2-ethoxybenzol

Downstream raw materials:

4-(4-ethoxy-3-propylphenyl)-4-oxobutanoic acid