4-(4,9-diethoxy-1-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzyl methanesulfonate

Base Information

Chemical Name:4-(4,9-diethoxy-1-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzyl methanesulfonate
CAS No.:1064195-74-9
Molecular Formula:C₂₅H₂₇NO₆S
Molecular Weight:469.558
Hs Code.:

Synonyms:4-(4,9-diethoxy-1-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzyl methanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(4,9-diethoxy-1-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzyl methanesulfonate

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Technology Process of 4-(4,9-diethoxy-1-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzyl methanesulfonate

There total 9 articles about 4-(4,9-diethoxy-1-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1064195-73-8
4,9-diethoxy-2-[4-(hydroxymethyl)-2-methylphenyl]-2,3-dihydro-1H-benzo[f]isoindol-1-one

: 124-63-0
methanesulfonyl chloride

: 1064195-74-9
4-(4,9-diethoxy-1-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzyl methanesulfonate

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2010.12.014

Reference yield:

: 1064195-70-5
methyl 4-(4,9-diethoxy-1-hydroxy-3-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzoate

: 1064195-74-9
4-(4,9-diethoxy-1-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzyl methanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylsilane; trifluoroacetic acid / dichloromethane

2: water; lithium hydroxide / tetrahydrofuran; methanol

3: dimethylsulfide borane complex / tetrahydrofuran

4: triethylamine / dichloromethane

With triethylsilane; dimethylsulfide borane complex; water; triethylamine; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2010.12.014

Reference yield:

: 1064195-71-6
methyl 4-(4,9-diethoxy-1-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzoate

: 1064195-74-9
4-(4,9-diethoxy-1-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzyl methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: water; lithium hydroxide / tetrahydrofuran; methanol

2: dimethylsulfide borane complex / tetrahydrofuran

3: triethylamine / dichloromethane

With dimethylsulfide borane complex; water; triethylamine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2010.12.014