CH₃OB(C₆H₄CH₂NHC₆H₁₁)2

Base Information

Chemical Name:CH₃OB(C₆H₄CH₂NHC₆H₁₁)2
CAS No.:1159250-76-6
Molecular Formula:C₂₇H₃₉BN₂O
Molecular Weight:418.43
Hs Code.:

CH<sub>3</sub>OB(C<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>NHC<sub>6</sub>H<sub>11</sub>)2

Synonyms:CH₃OB(C₆H₄CH₂NHC₆H₁₁)2

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Chemical Property of CH₃OB(C₆H₄CH₂NHC₆H₁₁)2

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Technology Process of CH₃OB(C₆H₄CH₂NHC₆H₁₁)2

There total 2 articles about CH₃OB(C₆H₄CH₂NHC₆H₁₁)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 121-43-7,63156-11-6
Trimethyl borate

: 356531-41-4
N-(2-bromobenzyl)cyclohexanamine

: 1159250-76-6
CH₃OB(C₆H₄CH₂NHC₆H₁₁)2

Guidance literature:: With n-butyllithium; In diethyl ether; to o-BrC6H4CH2NHCy n-BuLi in hexane was added at -44°C and stirred for 1 h, heated to room temp., B(OMe)3 was added at room temp. (2:4:1), stirred for 12 h, CH2Cl2 was added; hexane was added, ppt. was filtered and recrystd. from CHCl3-MeOH;
DOI:10.1021/ja9029494