ethyl 3-(7-(2-chlorophenoxy)-1-cyano-4-hydroxyisoquinoline-3-carboxamido)-2,2-dimethylpropanoate

Base Information

Chemical Name:ethyl 3-(7-(2-chlorophenoxy)-1-cyano-4-hydroxyisoquinoline-3-carboxamido)-2,2-dimethylpropanoate
CAS No.:1455092-35-9
Molecular Formula:C₂₄H₂₂ClN₃O₅
Molecular Weight:467.909
Hs Code.:

Synonyms:ethyl 3-(7-(2-chlorophenoxy)-1-cyano-4-hydroxyisoquinoline-3-carboxamido)-2,2-dimethylpropanoate

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Chemical Property of ethyl 3-(7-(2-chlorophenoxy)-1-cyano-4-hydroxyisoquinoline-3-carboxamido)-2,2-dimethylpropanoate

Chemical Property:

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Technology Process of ethyl 3-(7-(2-chlorophenoxy)-1-cyano-4-hydroxyisoquinoline-3-carboxamido)-2,2-dimethylpropanoate

There total 3 articles about ethyl 3-(7-(2-chlorophenoxy)-1-cyano-4-hydroxyisoquinoline-3-carboxamido)-2,2-dimethylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59193-77-0
3-amino-2,2-dimethylpropionic acid ethyl ester

: 1455092-32-6
methyl 7-(2-chlorophenoxy)-1-cyano-4-hydroxyisoquinoline-3-carboxylate

: 1455092-35-9
ethyl 3-(7-(2-chlorophenoxy)-1-cyano-4-hydroxyisoquinoline-3-carboxamido)-2,2-dimethylpropanoate

Guidance literature:: In ethanol; at 150 ℃; for 1.5h; Microwave irradiation;

Reference yield:

: 1572-98-1
2-cyano-2-methyl-propionic acid ethyl ester

: 1455092-35-9
ethyl 3-(7-(2-chlorophenoxy)-1-cyano-4-hydroxyisoquinoline-3-carboxamido)-2,2-dimethylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / ethanol / 20 h / 20 °C

2: ethanol / 1.5 h / 150 °C / Microwave irradiation

With hydrogen; In ethanol;

Reference yield:

: methyl 7-(2-chlorophenoxy)-4-hydroxy-1-iodoisoquinoline-3-carboxylate

: 1455092-35-9
ethyl 3-(7-(2-chlorophenoxy)-1-cyano-4-hydroxyisoquinoline-3-carboxamido)-2,2-dimethylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 0.12 h / 120 °C

2: ethanol / 1.5 h / 150 °C / Microwave irradiation

In ethanol; N,N-dimethyl-formamide;