RARECHEM AL BW 0424

Base Information

• Chemical Name: RARECHEM AL BW 0424
• CAS No.: 59193-77-0
• Molecular Formula: C7H15NO2
• Molecular Weight: 145.202
• Mol file: 59193-77-0.mol

Synonyms:Ethyl 3-amino-2,2-dimethylpropanoate;

Chemical Property of RARECHEM AL BW 0424

Chemical Property:

• Boiling Point: 192.277 °C at 760 mmHg
• PKA: 8.88±0.10(Predicted)
• Flash Point: 63.701 °C
• PSA: 52.32000
• Density: 0.96 g/cm³
• LogP: 1.23470
• Storage Temp.: Keep in dark place,Inert atmosphere,Store in freezer, under -20°C

Purity/Quality:

97% ^*data from raw suppliers

Ethyl3-amino-2,2-dimethylpropanoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of RARECHEM AL BW 0424

There total 4 articles about RARECHEM AL BW 0424 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-cyano-2-methyl-propionic acid ethyl ester (1572-98-1) → 3-amino-2,2-dimethylpropionic acid ethyl ester (59193-77-0)

Guidance literature:

With ammonia; hydrogen; 5% Rh/Al2O3; In ethanol; at 20 ℃; for 40h;

Reference yield:

3-bromo-2,2-dimethylpropionic acid (2843-17-6) + ethanol (64-17-5) → 3-amino-2,2-dimethylpropionic acid ethyl ester (59193-77-0)

Guidance literature:

3-bromo-2,2-dimethylpropionic acid; With ammonia; In water; at 0 - 55 ℃; for 72h; Sealed high-pressure vessel;

ethanol; With thionyl chloride; at 0 - 20 ℃; Heating / reflux;

Reference yield:

ethanol (64-17-5) + aminopivalic acid (19036-43-2) → 3-amino-2,2-dimethylpropionic acid ethyl ester (59193-77-0)

Guidance literature:

ethanol; aminopivalic acid; With thionyl chloride; at 0 - 90 ℃; for 6h;

With ammonium hydroxide; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/acs.joc.0c00115

upstream raw materials:

2-cyano-2-methyl-propionic acid ethyl ester

3-bromo-2,2-dimethylpropionic acid

ethanol

aminopivalic acid

Downstream raw materials:

3,3-dimethyl-2-azetidinone

aminopivalic acid

3-(Tosylamino)pivalinsaeure

ethyl 2,2-dimethyl-3-[(2-methylpropan-2-yl)oxycarbonylamino]propanoate

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