trans-Pd(PPh₃)2(Cl)(COPh)

Base Information

Chemical Name:trans-Pd(PPh₃)2(Cl)(COPh)
CAS No.:111772-04-4
Molecular Formula:C₄₃H₃₅ClOP₂Pd
Molecular Weight:863.975
Hs Code.:

Synonyms:trans-Pd(PPh₃)2(Cl)(COPh)

Suppliers and Price of trans-Pd(PPh₃)2(Cl)(COPh)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of trans-Pd(PPh₃)2(Cl)(COPh)

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of trans-Pd(PPh₃)2(Cl)(COPh)

There total 16 articles about trans-Pd(PPh₃)2(Cl)(COPh) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 14104-20-2
silver tetrafluoroborate

: 111772-04-4
trans-Pd(PPh₃)2(Cl)(COPh)

: 111772-04-4
trans-{Pd(PPh₃)2(CH₃CN)(COPh)}(BF₄)

Guidance literature:: With acetonitrile; In dichloromethane; acetonitrile; byproducts: AgCl; prep. under N2 in a 10:1 (vol/vol) mixt. of CH2Cl2/CH3CN, rapid stirring, dropwise addn. of AgBF4-soln. (CH3CN); pptn. in Et2O at 0 °C, filtration, washing with Et2O and pentane, drying under vacuum;
DOI:10.1021/ja00211a020

Reference yield: 93.0%

: 14221-01-3
tetrakis(triphenylphosphine) palladium⁽⁰⁾

: 98-88-4
benzoyl chloride

: 111772-04-4
trans-Pd(PPh₃)2(Cl)(COPh)

Guidance literature:: under N2;
DOI:10.1021/ja00211a020

Reference yield: 93.0%

: 14104-20-2
silver tetrafluoroborate

: 111772-04-4
trans-Pd(PPh₃)2(Cl)(COPh)

: 75-05-8,26809-02-9
acetonitrile

: 111772-04-4
trans-{Pd(PPh₃)2(CH₃CN)(COPh)}(BF₄)

Guidance literature:: In dichloromethane; acetonitrile; byproducts: silver chloride; (dry N2); dry and deoxygenated solvents; dissolving Pd-compd. in CH2Cl2/CH3CN 10:1, addn. of 1 equiv. of AgBF4 in CH3CN to the stirring soln. dropwise; filtration, pptn. on addn. filtrate to stirring Et2O soln. at 0°C, filtration, washing (ether, pentane), drying in vac.;
DOI:10.1021/om00156a010