(E)-methyl <3-<2-cyano-2-(4,5-diphenyl-2-oxazolyl)ethenyl>phenoxy>acetate

Base Information

Chemical Name:(E)-methyl <3-<2-cyano-2-(4,5-diphenyl-2-oxazolyl)ethenyl>phenoxy>acetate
CAS No.:147594-34-1
Molecular Formula:C₂₇H₂₀N₂O₄
Molecular Weight:436.467
Hs Code.:

Synonyms:(E)-methyl <3-<2-cyano-2-(4,5-diphenyl-2-oxazolyl)ethenyl>phenoxy>acetate

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Chemical Property of (E)-methyl <3-<2-cyano-2-(4,5-diphenyl-2-oxazolyl)ethenyl>phenoxy>acetate

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Technology Process of (E)-methyl <3-<2-cyano-2-(4,5-diphenyl-2-oxazolyl)ethenyl>phenoxy>acetate

There total 2 articles about (E)-methyl <3-<2-cyano-2-(4,5-diphenyl-2-oxazolyl)ethenyl>phenoxy>acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 37748-10-0
methyl (3-formylphenoxy)acetate

: 65913-22-6
2-(4,5-diphenyloxazol-2-yl)acetonitrile

: 147594-34-1
(E)-methyl <3-<2-cyano-2-(4,5-diphenyl-2-oxazolyl)ethenyl>phenoxy>acetate

Guidance literature:: With piperidine; toluene-4-sulfonic acid; In toluene; for 18h; Heating;
DOI:10.1021/jm00076a017

Reference yield:

: 81819-14-9
(4,5-diphenyloxazol-2-yl)methyl bromide

: 147594-34-1
(E)-methyl <3-<2-cyano-2-(4,5-diphenyl-2-oxazolyl)ethenyl>phenoxy>acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 32 percent / 18-crown-6 / CH₂Cl₂; H₂O / 25 h / Ambient temperature

2: 59 percent / piperidine, p-TsOH / toluene / 18 h / Heating

With piperidine; 18-crown-6 ether; toluene-4-sulfonic acid; In dichloromethane; water; toluene;
DOI:10.1021/jm00076a017