2-{3'-(tert-butoxycarbonylamino)-5'-[13''-(3'''-(tert-butyldimethylsilyloxy)-17'''β-(tetrahydro-2H-pyran-2-yl-oxy)-estra-1''',3''',5'''(10''')-trien-16β-yl)tridec-1-ynyl]phenyl}ethyl alcohol

Base Information

Chemical Name:2-{3'-(tert-butoxycarbonylamino)-5'-[13''-(3'''-(tert-butyldimethylsilyloxy)-17'''β-(tetrahydro-2H-pyran-2-yl-oxy)-estra-1''',3''',5'''(10''')-trien-16β-yl)tridec-1-ynyl]phenyl}ethyl alcohol
CAS No.:1191446-84-0
Molecular Formula:C₅₅H₈₅NO₆Si
Molecular Weight:884.368
Hs Code.:

2-{3'-(tert-butoxycarbonylamino)-5'-[13''-(3'''-(tert-butyldimethylsilyloxy)-17'''β-(tetrahydro-2H-pyran-2-yl-oxy)-estra-1''',3''',5'''(10''')-trien-16β-yl)tridec-1-ynyl]phenyl}ethyl alcohol

Synonyms:2-{3'-(tert-butoxycarbonylamino)-5'-[13''-(3'''-(tert-butyldimethylsilyloxy)-17'''β-(tetrahydro-2H-pyran-2-yl-oxy)-estra-1''',3''',5'''(10''')-trien-16β-yl)tridec-1-ynyl]phenyl}ethyl alcohol

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Chemical Property of 2-{3'-(tert-butoxycarbonylamino)-5'-[13''-(3'''-(tert-butyldimethylsilyloxy)-17'''β-(tetrahydro-2H-pyran-2-yl-oxy)-estra-1''',3''',5'''(10''')-trien-16β-yl)tridec-1-ynyl]phenyl}ethyl alcohol

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Technology Process of 2-{3'-(tert-butoxycarbonylamino)-5'-[13''-(3'''-(tert-butyldimethylsilyloxy)-17'''β-(tetrahydro-2H-pyran-2-yl-oxy)-estra-1''',3''',5'''(10''')-trien-16β-yl)tridec-1-ynyl]phenyl}ethyl alcohol

There total 1 articles about 2-{3'-(tert-butoxycarbonylamino)-5'-[13''-(3'''-(tert-butyldimethylsilyloxy)-17'''β-(tetrahydro-2H-pyran-2-yl-oxy)-estra-1''',3''',5'''(10''')-trien-16β-yl)tridec-1-ynyl]phenyl}ethyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 766543-59-3
methyl 2-{3'-(tert-butoxycarbonylamino)-5'-[13''-(3'''-(tert-butyldimethylsilyloxy)-17'''β-(tetrahydro-2H-pyran-2-yl-oxy)-estra-1''',3''',5'''(10''')-trien-16'''β-yl)-tridecynyl]-phenyl}-acetate

: 1191446-84-0
2-{3'-(tert-butoxycarbonylamino)-5'-[13''-(3'''-(tert-butyldimethylsilyloxy)-17'''β-(tetrahydro-2H-pyran-2-yl-oxy)-estra-1''',3''',5'''(10''')-trien-16β-yl)tridec-1-ynyl]phenyl}ethyl alcohol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1139/V09-083

Reference yield: 82.0%

: 1191446-84-0
2-{3'-(tert-butoxycarbonylamino)-5'-[13''-(3'''-(tert-butyldimethylsilyloxy)-17'''β-(tetrahydro-2H-pyran-2-yl-oxy)-estra-1''',3''',5'''(10''')-trien-16β-yl)tridec-1-ynyl]phenyl}ethyl alcohol

: 121-45-9
phosphorous acid trimethyl ester

: 1191446-86-2
dimethyl 2-{3'-(tert-butoxycarbonylamino)-5'-[13''-(3'''-(tert-butyldimethylsilyloxy)-17'''β-(tetrahydro-2H-pyran-2-yl-oxy)-estra-1''',3''',5'''(10''')-trien-16'''β-yl)tridec-1-ynyl]phenyl}ethyl phosphate

Guidance literature:: With pyridine; carbon tetrabromide; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1139/V09-083

Reference yield: 70.0%

: 1191446-84-0
2-{3'-(tert-butoxycarbonylamino)-5'-[13''-(3'''-(tert-butyldimethylsilyloxy)-17'''β-(tetrahydro-2H-pyran-2-yl-oxy)-estra-1''',3''',5'''(10''')-trien-16β-yl)tridec-1-ynyl]phenyl}ethyl alcohol

: C₅₀H₇₆BrNO₄Si

: 1191446-85-1
2-{3'-(tert-butoxycarbonylamino)-5'-[13''-(3'''-(tert-butyldimethylsilyloxy)-17'''β-(tetrahydro-2H-pyran-2-yl-oxy)-estra-1''',3''',5'''(10''')-trien-16β-yl)tridec-1-ynyl]phenyl}ethyl bromide

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 0 ℃; for 3.5h; Inert atmosphere;
DOI:10.1139/V09-083