4-(tert-butyldimethylsilyloxy)-N₁-(6-indolylcarbonyl)-N₂-[1-(pyridin-4-yl)piperidin-4-yl]methoxycarbonyl-1,2-benzenediamine

Base Information

• Chemical Name: 4-(tert-butyldimethylsilyloxy)-N₁-(6-indolylcarbonyl)-N₂-[1-(pyridin-4-yl)piperidin-4-yl]methoxycarbonyl-1,2-benzenediamine
• CAS No.: 219508-15-3
• Molecular Formula: C₃₃H₄₁N₅O₄Si
• Molecular Weight: 599.805

Synonyms:4-(tert-butyldimethylsilyloxy)-N₁-(6-indolylcarbonyl)-N₂-[1-(pyridin-4-yl)piperidin-4-yl]methoxycarbonyl-1,2-benzenediamine

Chemical Property of 4-(tert-butyldimethylsilyloxy)-N₁-(6-indolylcarbonyl)-N₂-[1-(pyridin-4-yl)piperidin-4-yl]methoxycarbonyl-1,2-benzenediamine

Chemical Property:

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Technology Process of 4-(tert-butyldimethylsilyloxy)-N₁-(6-indolylcarbonyl)-N₂-[1-(pyridin-4-yl)piperidin-4-yl]methoxycarbonyl-1,2-benzenediamine

There total 1 articles about 4-(tert-butyldimethylsilyloxy)-N₁-(6-indolylcarbonyl)-N₂-[1-(pyridin-4-yl)piperidin-4-yl]methoxycarbonyl-1,2-benzenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Indole-6-carboxylic acid (1670-82-2,261352-47-0) + 4-(tert-butyldimethylsilyloxy)-N2-[1-(4-pyridyl)piperidin-4-yl]methoxycarbonyl-1,2-benzenediamine (219492-56-5) + sodium hydrogencarbonate (144-55-8) + bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate (132705-51-2) → 4-(tert-butyldimethylsilyloxy)-N1-(6-indolylcarbonyl)-N2-[1-(pyridin-4-yl)piperidin-4-yl]methoxycarbonyl-1,2-benzenediamine (219508-15-3)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

4-(tert-butyldimethylsilyloxy)-N1-(6-indolylcarbonyl)-N2-[1-(pyridin-4-yl)piperidin-4-yl]methoxycarbonyl-1,2-benzenediamine (219508-15-3) → 4-Hydroxy-N1-(6-indolylcarbonyl)-N2-[1-(pyridin-4-yl)piperidin-4-yl]methoxycarbonyl-1,2-benzenediamine (219507-50-3)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran;

Reference yield:

4-(tert-butyldimethylsilyloxy)-N1-(6-indolylcarbonyl)-N2-[1-(pyridin-4-yl)piperidin-4-yl]methoxycarbonyl-1,2-benzenediamine (219508-15-3) + 1,1'-azobis (cyclohexanecarbonitrile) (2094-98-6) → hydrated HCl salt + 4-Hydroxy-N1-(6-indolylcarbonyl)-N2-[l-(4-pyridyl)piperidin-4-yl]methoxycarbonyl-1,2-benzenediamine hydrochloride hydrate

Guidance literature:

With hydrogenchloride; In tetrahydrofuran;

upstream raw materials:

Indole-6-carboxylic acid

4-(tert-butyldimethylsilyloxy)-N₂-[1-(4-pyridyl)piperidin-4-yl]methoxycarbonyl-1,2-benzenediamine

sodium hydrogencarbonate

bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate

Downstream raw materials:

4-Hydroxy-N₁-(6-indolylcarbonyl)-N₂-[1-(pyridin-4-yl)piperidin-4-yl]methoxycarbonyl-1,2-benzenediamine

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