benzyl 4-((4-(trifluoromethylsulfonyloxy)cyclohex-3-enyloxy)methyl)piperidine-1-carboxylate

Base Information

Chemical Name:benzyl 4-((4-(trifluoromethylsulfonyloxy)cyclohex-3-enyloxy)methyl)piperidine-1-carboxylate
CAS No.:1401098-36-9
Molecular Formula:C₂₁H₂₆F₃NO₆S
Molecular Weight:477.502
Hs Code.:

Synonyms:benzyl 4-((4-(trifluoromethylsulfonyloxy)cyclohex-3-enyloxy)methyl)piperidine-1-carboxylate

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Chemical Property of benzyl 4-((4-(trifluoromethylsulfonyloxy)cyclohex-3-enyloxy)methyl)piperidine-1-carboxylate

Chemical Property:

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Technology Process of benzyl 4-((4-(trifluoromethylsulfonyloxy)cyclohex-3-enyloxy)methyl)piperidine-1-carboxylate

There total 3 articles about benzyl 4-((4-(trifluoromethylsulfonyloxy)cyclohex-3-enyloxy)methyl)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 1401098-35-8
benzyl 4-((4-oxocyclohexyloxy)methyl)piperidine-1-carboxylate

: 1401098-36-9
benzyl 4-((4-(trifluoromethylsulfonyloxy)cyclohex-3-enyloxy)methyl)piperidine-1-carboxylate

Guidance literature:: benzyl 4-((4-oxocyclohexyloxy)methyl)piperidine-1-carboxylate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

N,N-phenylbistrifluoromethane-sulfonimide; In tetrahydrofuran; at -78 - 20 ℃; for 1.5h;

Reference yield:

: 22428-87-1
4,4-ethylenedioxycyclohexan-1-ol

: 1401098-36-9
benzyl 4-((4-(trifluoromethylsulfonyloxy)cyclohex-3-enyloxy)methyl)piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 20 °C

1.2: 1 h / 100 °C / Microwave irradiation

2.1: hydrogenchloride / tetrahydrofuran / 25 h / 20 - 40 °C

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

3.2: 1.5 h / -78 - 20 °C

With hydrogenchloride; sodium hydride; lithium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1401098-34-7
benzyl 4-((1,4-dioxaspiro[4.5]decan-8-yloxy)methyl)piperidine-1-carboxylate

: 1401098-36-9
benzyl 4-((4-(trifluoromethylsulfonyloxy)cyclohex-3-enyloxy)methyl)piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / tetrahydrofuran / 25 h / 20 - 40 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 1.5 h / -78 - 20 °C

With hydrogenchloride; lithium hexamethyldisilazane; In tetrahydrofuran;