[BzPh₃P][^tBuDTO]

Base Information

Chemical Name:[BzPh₃P][^tBuDTO]
CAS No.:1318259-07-2
Molecular Formula:C₆H₉O₂S₂*C₂₅H₂₂P
Molecular Weight:530.692
Hs Code.:

Synonyms:[BzPh₃P][^tBuDTO]

Suppliers and Price of [BzPh₃P][^tBuDTO]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [BzPh₃P][^tBuDTO]

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [BzPh₃P][^tBuDTO]

There total 1 articles about [BzPh₃P][^tBuDTO] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 107-59-5
tert-Butyl chloroacetate

: 1100-88-5
benzyltriphenylphosphonium chloride

: 1318259-07-2
[BzPh₃P][^tBuDTO]

Guidance literature:: tert-Butyl chloroacetate; With sulfur; triethylamine; In N,N-dimethyl-formamide; at 20 - 30 ℃; for 2h;

benzyltriphenylphosphonium chloride; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ica.2011.02.037

Reference yield: 84.0%

: 15709-76-9
tris(triphenylphosphino)copper(I) chloride

: 1318259-07-2
[BzPh₃P][^tBuDTO]

: 1318259-09-4
Cu(P(C6H5)3)2(η2-O-t-butyl-1,1-dithiooxalate)

Guidance literature:: In dichloromethane; synthesis according to P.Strauch et al. Z. Anorg. Allg. Chem. 620 (1994), 498: to soln. of Cu-complex soln. of dithiooxalate added dropwise over5 min, covered with watch glass, stirred in dark for 1 h; solvent removed (reduced pressure), residue recrystd. twice from CH2Cl2/i-PrOH at -20 °C;
DOI:10.1016/j.ica.2011.02.037

Reference yield: 60.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 1318259-07-2
[BzPh₃P][^tBuDTO]

: 7789-45-9
copper(ll) bromide

: (PPh₃Bz)(O-t-butyl-1-perthio-1-thiooxalato)CuBr*0.5C₄H₈O

Guidance literature:: In dichloromethane; water; (Ar); soln. of dithiooxalate in CH2Cl2 added slowly to stirred deaeratedaq. soln. of CuBr2, aq. phase removed after 30 min of stirring, organic layer concd. (vac.), solid washed (THF); gravity filtered through glass wool packed Pasture pipette, diethyl ether slowly diffused, ppt. washed (Et2O), recrystd.; elem. anal.;
DOI:10.1016/j.ica.2011.02.037