Technology Process of 1,1,1,3,3,3-hexafluoropropan-2-yl 3,3-diphenylpropanoate
There total 3 articles about 1,1,1,3,3,3-hexafluoropropan-2-yl 3,3-diphenylpropanoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate;
at 20 ℃;
Sealed tube;
DOI:10.1021/ol400785d
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate; sodium hypochlorite / dichloromethane; water / 1 h / 20 °C
2: 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate; pyridine / 20 °C / Sealed tube
With
pyridine; sodium hypochlorite; 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate;
In
dichloromethane; water;
DOI:10.1021/ol400785d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium aluminium tetrahydride / diethyl ether; tetrahydrofuran / 2 h / 0 °C / Inert atmosphere; Schlenk technique; Sealed tube
2: 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate; sodium hypochlorite / dichloromethane; water / 1 h / 20 °C
3: 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate; pyridine / 20 °C / Sealed tube
With
pyridine; sodium hypochlorite; lithium aluminium tetrahydride; 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate;
In
tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1021/ol400785d
