N-(4-nitrophenyl)-N'-acetylthiourea

Base Information

Chemical Name:N-(4-nitrophenyl)-N'-acetylthiourea
CAS No.:66934-12-1
Molecular Formula:C₉H₉N₃O₃S
Molecular Weight:239.255
Hs Code.:

Synonyms:N-(4-nitrophenyl)-N'-acetylthiourea

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Chemical Property of N-(4-nitrophenyl)-N'-acetylthiourea

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Technology Process of N-(4-nitrophenyl)-N'-acetylthiourea

There total 4 articles about N-(4-nitrophenyl)-N'-acetylthiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 333-20-0
potassium thioacyanate

: 100-01-6,104810-17-5
4-nitro-aniline

: 75-36-5
acetyl chloride

: 66934-12-1
N-(4-nitrophenyl)-N'-acetylthiourea

Guidance literature:: potassium thioacyanate; acetyl chloride; In water; acetone; for 3h;

4-nitro-aniline; In water; acetone; for 5h; Reflux;
DOI:10.1016/j.molstruc.2015.06.024

Reference yield:

: 1147550-11-5
ammonium thiocyanate

: 100-01-6,104810-17-5
4-nitro-aniline

: 75-36-5
acetyl chloride

: 66934-12-1
N-(4-nitrophenyl)-N'-acetylthiourea

Guidance literature:: ammonium thiocyanate; acetyl chloride; With PEG-400; In dichloromethane; at 20 ℃; for 3h;

4-nitro-aniline; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.cclet.2015.08.001