Cyclohexanecarboxamide, 2-amino-, (1R,2R)-rel- (9CI)

Base Information Edit

Chemical Name:Cyclohexanecarboxamide, 2-amino-, (1R,2R)-rel- (9CI)
CAS No.:110901-40-1
Molecular Formula:C7H14 N2 O
Molecular Weight:142.201
Hs Code.:
Mol file:110901-40-1.mol

Synonyms:Cyclohexanecarboxamide,2-amino-, trans-; trans-2-Aminocyclohexanecarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexanecarboxamide, 2-amino-, (1R,2R)-rel- (9CI) Edit

Chemical Property:

Melting Point:156-159 °C(Solv: ethanol (64-17-5))
Boiling Point:321.8±31.0 °C(Predicted)
PKA:16.65±0.40(Predicted)
PSA：69.11000
Density:1.073±0.06 g/cm3(Predicted)
LogP:1.38980

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclohexanecarboxamide, 2-amino-, (1R,2R)-rel- (9CI)

There total 4 articles about Cyclohexanecarboxamide, 2-amino-, (1R,2R)-rel- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 132724-02-8
trans-2-(benzyloxycarbonylamino)cyclohexanecarboxamide

: 110901-40-1,115014-77-2
trans-2-aminocyclohexane-1-carboxamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 22 ℃; under 760 Torr;

Reference yield: 64.0%

: 1436-60-8,1436-61-9,24716-94-7,26849-62-7,64162-07-8,75197-07-8,115014-75-0
ethyl cis-2-amino-1-cyclohexanecarboxylate

: 110901-40-1,115014-77-2
trans-2-aminocyclohexane-1-carboxamide

Guidance literature:: With ammonia; In methanol; for 504h; Ambient temperature;

Reference yield:

: 5691-19-0
trans-2-amino-1-cyclohexanecarboxylic acid

: 110901-40-1,115014-77-2
trans-2-aminocyclohexane-1-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) aq. 2 N NaOH, 2.) aq. 2 N NaOH / 2.) 4 h

2: 1.) triethylamine, isobutyl chloroformate, 2.) NH₃ / 1.) THF, -10 deg, 15 min., 2.) a) -10 deg C, 5 h, b) r.t., 12 h

3: 95 percent / H₂ / 10percent Pd/C / ethanol / 22 °C / 760 Torr

With sodium hydroxide; ammonia; hydrogen; triethylamine; isobutyl chloroformate; palladium on activated charcoal; In ethanol;