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Technology Process of [(HC(C(tBu)NC6H3(iPr)2)2)Ni(diethyl ether)]

[(HC(C(tBu)NC6H3(iPr)2)2)Ni(diethyl ether)]

Base Information
  • Chemical Name:[(HC(C(tBu)NC6H3(iPr)2)2)Ni(diethyl ether)]
  • CAS No.:1163771-25-2
  • Molecular Formula:C39H63N2NiO
  • Molecular Weight:634.632
  • Hs Code.:
[(HC(C(<sup>t</sup>Bu)NC<sub>6</sub>H<sub>3</sub>(iPr)<sub>2</sub>)<sub>2</sub>)Ni(diethyl ether)]

Synonyms:[(HC(C(tBu)NC6H3(iPr)2)2)Ni(diethyl ether)]

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Chemical Property of [(HC(C(tBu)NC6H3(iPr)2)2)Ni(diethyl ether)]
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Technology Process of [(HC(C(tBu)NC6H3(iPr)2)2)Ni(diethyl ether)]

There total 2 articles about [(HC(C(tBu)NC6H3(iPr)2)2)Ni(diethyl ether)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl ether
60-29-7,927820-24-4

diethyl ether

[([HC(C(<sup>t</sup>Bu)NC<sub>6</sub>H<sub>3</sub>(iPr)<sub>2</sub>)<sub>2</sub>])Ni(Br)]
1163771-26-3

[([HC(C(tBu)NC6H3(iPr)2)2])Ni(Br)]

[(HC(C(<sup>t</sup>Bu)NC<sub>6</sub>H<sub>3</sub>(iPr)<sub>2</sub>)<sub>2</sub>)Ni(diethyl ether)]
1163771-25-2

[(HC(C(tBu)NC6H3(iPr)2)2)Ni(diethyl ether)]

Guidance literature:
With KC8; In hexane; (inert atm.); treatment of nickel compd. with KC8 in hexane; isolation of ppt., extn. (diethyl ether);
DOI:10.1021/om9007983

Reference yield:

diethyl ether
60-29-7,927820-24-4

diethyl ether

[((HC(CtBuNC<sub>6</sub>H<sub>3</sub>(iPr)<sub>2</sub>)<sub>2</sub>)Ni<sup>I</sup>)<sub>2</sub>(μ-η<sup>1</sup>:η<sup>1</sup>-N<sub>2</sub>)]
1163771-24-1

[((HC(CtBuNC6H3(iPr)2)2)NiI)2(μ-η1:η1-N2)]

[(HC(C(<sup>t</sup>Bu)NC<sub>6</sub>H<sub>3</sub>(iPr)<sub>2</sub>)<sub>2</sub>)Ni(diethyl ether)]
1163771-25-2

[(HC(C(tBu)NC6H3(iPr)2)2)Ni(diethyl ether)]

Guidance literature:
In diethyl ether; byproducts: N2; (Ar), using glove box or Schlenk technique; react. of Ni complex with Et2O;

Reference yield: 78.0%

[(HC(C(<sup>t</sup>Bu)NC<sub>6</sub>H<sub>3</sub>(iPr)<sub>2</sub>)<sub>2</sub>)Ni(diethyl ether)]
1163771-25-2

[(HC(C(tBu)NC6H3(iPr)2)2)Ni(diethyl ether)]

phenylhydrazine
100-63-0

phenylhydrazine

[(HC(C(<sup>t</sup>Bu)NC<sub>6</sub>H<sub>3</sub>(iPr)<sub>2</sub>)<sub>2</sub>)Ni(η<sup>2</sup>-phenylhydrazido(1-))]

[(HC(C(tBu)NC6H3(iPr)2)2)Ni(η2-phenylhydrazido(1-))]

Guidance literature:
In diethyl ether; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ic301066x
upstream raw materials:

diethyl ether

[((HC(CtBuNC6H3(iPr)2)2)NiI)2(μ-η1:η1-N2)]

[([HC(C(tBu)NC6H3(iPr)2)2])Ni(Br)]

Downstream raw materials:

[((HC(CtBuNC6H3(iPr)2)2)NiI)2(μ-η1:η1-N2)]

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