2-(2-fluorophenyl)-N-[(6-oxo-1,6-dihydropyridazin-3-yl)methyl]acetamide

Base Information

Chemical Name:2-(2-fluorophenyl)-N-[(6-oxo-1,6-dihydropyridazin-3-yl)methyl]acetamide
CAS No.:1407814-88-3
Molecular Formula:C₁₃H₁₂FN₃O₂
Molecular Weight:261.256
Hs Code.:

Synonyms:2-(2-fluorophenyl)-N-[(6-oxo-1,6-dihydropyridazin-3-yl)methyl]acetamide

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Chemical Property of 2-(2-fluorophenyl)-N-[(6-oxo-1,6-dihydropyridazin-3-yl)methyl]acetamide

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Technology Process of 2-(2-fluorophenyl)-N-[(6-oxo-1,6-dihydropyridazin-3-yl)methyl]acetamide

There total 5 articles about 2-(2-fluorophenyl)-N-[(6-oxo-1,6-dihydropyridazin-3-yl)methyl]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 1407814-85-0
2-(2-fluorophenyl)-N-[(6-oxo-1,4,5,6-tetrahydropyridazin-3-yl)methyl]acetamide

: 1407814-88-3
2-(2-fluorophenyl)-N-[(6-oxo-1,6-dihydropyridazin-3-yl)methyl]acetamide

Guidance literature:: 2-(2-fluorophenyl)-N-[(6-oxo-1,4,5,6-tetrahydropyridazin-3-yl)methyl]acetamide; With bromine; In acetic acid; at 50 ℃; for 3h;

With sodium hydrogencarbonate; In water;

Reference yield: 25.0%

: 144-55-8
sodium hydrogencarbonate

: 1407814-88-3
2-(2-fluorophenyl)-N-[(6-oxo-1,6-dihydropyridazin-3-yl)methyl]acetamide

Guidance literature:: With bromine; In acetic acid;

Reference yield:

: 79416-27-6
methyl aminolevulinate

: 1407814-88-3
2-(2-fluorophenyl)-N-[(6-oxo-1,6-dihydropyridazin-3-yl)methyl]acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / ethanol / 0.75 h / Reflux

2: triethylamine / acetonitrile / 72 h / 0 - 20 °C / Molecular sieve

3: bromine / acetic acid / 3 h / 50 °C

With bromine; hydrazine hydrate; triethylamine; In ethanol; acetic acid; acetonitrile;