Acetic acid (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yl ester

Base Information

Chemical Name:Acetic acid (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yl ester
CAS No.:120316-50-9
Molecular Formula:C₃₅H₃₆O₆Se
Molecular Weight:631.627
Hs Code.:

Synonyms:Acetic acid (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yl ester

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Chemical Property of Acetic acid (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yl ester

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Technology Process of Acetic acid (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yl ester

There total 2 articles about Acetic acid (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5707-04-0
Phenylselenyl chloride

: 55628-54-1
3,4,6-tri-O-benzyl-D-glucal

: 120316-47-4
Acetic acid (2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yl ester

: 120316-50-9
Acetic acid (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yl ester

: Acetic acid (2R,3R,4R,5S,6S)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yl ester

Guidance literature:: Product distribution; ratio of products in the presence of different metal acetates in CH₂Cl₂ or toluene, 0 to 25 deg C_.;
DOI:10.1016/S0040-4039(01)80327-0

Reference yield:

: 5707-04-0
Phenylselenyl chloride

: 55628-54-1
3,4,6-tri-O-benzyl-D-glucal

: 563-63-3
silver(I) acetate

: 120316-47-4
Acetic acid (2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yl ester

: 120316-50-9
Acetic acid (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yl ester

Guidance literature:: Product distribution; multistep reaction;
DOI:10.1016/S0040-4020(97)00571-1

Reference yield: 92.0%

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 120316-50-9
Acetic acid (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yl ester

: 120316-63-4
C₆₁H₆₄O₁₀Se

: 120316-59-8
C₆₁H₆₄O₁₀Se

Guidance literature:: With 4 A molecular sieve; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1016/S0040-4039(01)80327-0