Benzyl-4,6-O-benzyliden-2-desoxy-2-(2',4'-dinitroanilino)-α-D-glucopyranosid

Base Information

Chemical Name:Benzyl-4,6-O-benzyliden-2-desoxy-2-(2',4'-dinitroanilino)-α-D-glucopyranosid
CAS No.:81429-62-1
Molecular Formula:C₂₆H₂₅N₃O₉
Molecular Weight:523.499
Hs Code.:

Synonyms:Benzyl-4,6-O-benzyliden-2-desoxy-2-(2',4'-dinitroanilino)-α-D-glucopyranosid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl-4,6-O-benzyliden-2-desoxy-2-(2',4'-dinitroanilino)-α-D-glucopyranosid

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Technology Process of Benzyl-4,6-O-benzyliden-2-desoxy-2-(2',4'-dinitroanilino)-α-D-glucopyranosid

There total 1 articles about Benzyl-4,6-O-benzyliden-2-desoxy-2-(2',4'-dinitroanilino)-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 13347-83-6
benzyl 4,6-O-benzylidene-2-amino-2-deoxy-α-D-glucopyranoside

: 70-34-8,65727-75-5
2,4-Dinitrofluorobenzene

: 81429-62-1
Benzyl-4,6-O-benzyliden-2-desoxy-2-(2',4'-dinitroanilino)-α-D-glucopyranosid

Guidance literature:: With sodium hydrogencarbonate; In ethanol; water; for 60h;

Reference yield: 86.0%

: 81429-62-1
Benzyl-4,6-O-benzyliden-2-desoxy-2-(2',4'-dinitroanilino)-α-D-glucopyranosid

: 124-63-0
methanesulfonyl chloride

: 73793-24-5
Benzyl-4,6-O-benzyliden-2-desoxy-2-(2',4'-dinitroanilino)-3-O-methylsulfonyl-α-D-glucopyranosid

Guidance literature:: In pyridine; for 12h;

Reference yield:

: 81429-62-1
Benzyl-4,6-O-benzyliden-2-desoxy-2-(2',4'-dinitroanilino)-α-D-glucopyranosid

: Benzyl-4,6-di-O-acetyl-2-azido-2,3-didesoxy-3-(2',4'-dinitroanilino)-α-D-altropyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / pyridine / 12 h

2: 31 percent / NaN₃ / dimethylformamide / 5 h / Heating

3: 1) 70percent acetic acid / 1) 80 deg C, 2 h, 2) pyridine, 24 h

With sodium azide; acetic acid; In pyridine; N,N-dimethyl-formamide;