Phenyl-methyl -hydroxybenzenebutanoate

Base Information

Chemical Name:Phenyl-methyl -hydroxybenzenebutanoate
CAS No.:109684-03-9
Molecular Formula:C17H18 O3
Molecular Weight:270.328
Hs Code.:
Mol file:109684-03-9.mol

Synonyms:Benzyl 2-hydroxy-4-phenylbutyrate;Phenyl-methyl -hydroxybenzenebutanoate

Suppliers and Price of Phenyl-methyl -hydroxybenzenebutanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
racBenzyl2-Hydroxy-4-phenylbutyrate
5mg
$ 155.00

Total 2 raw suppliers

Chemical Property of Phenyl-methyl -hydroxybenzenebutanoate

Chemical Property:

Vapor Pressure:4.77E-08mmHg at 25°C
Refractive Index:1.576
Boiling Point:426.9°C at 760 mmHg
Flash Point:177.2°C
PSA：60.36000
Density:1.156g/cm³
LogP:2.05560
Solubility.:Chloroform, Dichloromethane

Purity/Quality:

90% ^*data from raw suppliers

racBenzyl2-Hydroxy-4-phenylbutyrate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses An intermediate in the preparation of Benazepril metabolites

Technology Process of Phenyl-methyl -hydroxybenzenebutanoate

There total 6 articles about Phenyl-methyl -hydroxybenzenebutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 4263-93-8,111611-91-7
2-hydroxy-4-phenylbutanoic acid

: 100-39-0
benzyl bromide

: 109684-03-9
benzyl 2(R)-hydroxy-4-phenylbutyrate

Guidance literature:: With triethylamine; In ethyl acetate; for 16h; Heating;
DOI:10.1021/jm00105a066

Reference yield: 38.0%

: 93921-85-8
ethyl 2-hydroxy-4-phenylbutanoate

: 908093-98-1
diazodiphenylmethane

: [4S-[4α,7α(R*),12bβ]]-7-[[S-1-[carbodiphenylmethoxy]-3-phenylpropyl]amino]-1,2,3,4,6,7,8,12b-octahydro-9-nitro-6-oxopyrido[2,1-a][2]benzazepine-4-carboxylic acid, diphenylmethyl ester

: 109684-03-9
benzyl 2(R)-hydroxy-4-phenylbutyrate

Guidance literature:: With hydrogenchloride; lithium hydroxide; In methanol; hexane; dichloromethane; ethyl acetate;

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 109684-03-9
benzyl 2(R)-hydroxy-4-phenylbutyrate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) LDA / 1) THF, -60 deg C, 10 min

2: 89 percent / xylene / Heating

3: 1) ozone, 2) dimethyl sulfide / 1) -60 deg C, 2) room temperature

With dimethylsulfide; ozone; lithium diisopropyl amide; In xylene;
DOI:10.1021/jo00013a011