(4S,5S)-2-(4-tert-butyldimethylsilyloxymethyl-5-phenyloxazolin-2-yl)phenyl, phenyl selenide

Base Information

• Chemical Name: (4S,5S)-2-(4-tert-butyldimethylsilyloxymethyl-5-phenyloxazolin-2-yl)phenyl, phenyl selenide
• CAS No.: 314049-44-0
• Molecular Formula: C₂₈H₃₃NO₂SeSi
• Molecular Weight: 522.621

Synonyms:(4S,5S)-2-(4-tert-butyldimethylsilyloxymethyl-5-phenyloxazolin-2-yl)phenyl, phenyl selenide

Chemical Property of (4S,5S)-2-(4-tert-butyldimethylsilyloxymethyl-5-phenyloxazolin-2-yl)phenyl, phenyl selenide

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Technology Process of (4S,5S)-2-(4-tert-butyldimethylsilyloxymethyl-5-phenyloxazolin-2-yl)phenyl, phenyl selenide

There total 1 articles about (4S,5S)-2-(4-tert-butyldimethylsilyloxymethyl-5-phenyloxazolin-2-yl)phenyl, phenyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

diphenyl diselenide (1666-13-3) + (4S,5S)-4-tert-Butyldimethylsiloxymethyl-2,5-diphenyl-4,5-dihydro-1,3-oxazole (175477-26-6) → (4S,5S)-2-(4-tert-butyldimethylsilyloxymethyl-5-phenyloxazolin-2-yl)phenyl, phenyl selenide (314049-44-0)

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; hexane; cyclohexane; at 20 ℃; for 24h;

DOI:10.1016/S0022-328X(00)00488-5

Reference yield: 92.0%

(4S,5S)-2-(4-tert-butyldimethylsilyloxymethyl-5-phenyloxazolin-2-yl)phenyl, phenyl selenide (314049-44-0) → (4S,5S)-2-(4-hydroxymethyl-5-phenyloxazolin-2-yl)phenyl, phenyl selenide (314049-49-5)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/S0022-328X(00)00488-5

Reference yield: 92.0%

chloroamine-T (127-65-1) + (4S,5S)-2-(4-tert-butyldimethylsilyloxymethyl-5-phenyloxazolin-2-yl)phenyl, phenyl selenide (314049-44-0) → (4S,5S)-Se-[2-(4-tert-butyldimethylsilyloxymethyl-5-phenyloxazolin-2-yl)phenyl]-Se-phenyl-N-(p-toluenesulfonyl)selenimide

Guidance literature:

With MS₄A; In toluene; at 25 ℃; for 24h;

DOI:10.1016/S0022-328X(00)00488-5

upstream raw materials:

diphenyl diselenide

(4S,5S)-4-tert-Butyldimethylsiloxymethyl-2,5-diphenyl-4,5-dihydro-1,3-oxazole

Downstream raw materials:

(4S,5S)-2-(4-hydroxymethyl-5-phenyloxazolin-2-yl)phenyl, phenyl selenide

(4S,5S)-2-(4-methoxymethyl-5-phenyloxazolin-2-yl)phenyl, phenyl selenide

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