C₂₂H₁₇NO₂⁽¹⁸⁾OS

Base Information

Chemical Name:C₂₂H₁₇NO₂⁽¹⁸⁾OS
CAS No.:1315477-96-3
Molecular Formula:C₂₂H₁₇NO₃S
Molecular Weight:377.448
Hs Code.:

C<sub>22</sub>H<sub>17</sub>NO<sub>2</sub><sup>(18)</sup>OS

Synonyms:C₂₂H₁₇NO₂⁽¹⁸⁾OS

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Chemical Property of C₂₂H₁₇NO₂⁽¹⁸⁾OS

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Technology Process of C₂₂H₁₇NO₂⁽¹⁸⁾OS

There total 4 articles about C₂₂H₁₇NO₂⁽¹⁸⁾OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1238252-11-3
N-(2-(1-hydroxy-1-phenylprop-2-yn-1-yl)phenyl)-4-methylbenzenesulfonamide

: 1315477-96-3
C₂₂H₁₇NO₂⁽¹⁸⁾OS

Guidance literature:: With N-iodo-succinimide; 2-(dicyclohexylphosphino)-2',4',6'-triisopropylbiphenyl Au bis(trifluoromethylsulfonyl)imide; ¹⁸O-labeled water; In acetone; for 16h; Inert atmosphere; Reflux;
DOI:10.1021/jo201208e

Reference yield:

: 1859-71-8
2-(tosylamino)benzophenone

: 1315477-96-3
C₂₂H₁₇NO₂⁽¹⁸⁾OS

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 3 h / Reflux; Inert atmosphere

1.2: 0.17 h / 20 °C / Inert atmosphere; Saturated solution

2.1: N-iodo-succinimide; 2-(dicyclohexylphosphino)-2',4',6'-triisopropylbiphenyl Au bis(trifluoromethylsulfonyl)imide; ¹⁸O-labeled water / acetone / 16 h / Inert atmosphere; Reflux

With N-iodo-succinimide; 2-(dicyclohexylphosphino)-2',4',6'-triisopropylbiphenyl Au bis(trifluoromethylsulfonyl)imide; ¹⁸O-labeled water; In tetrahydrofuran; acetone;
DOI:10.1021/jo201208e

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1315477-96-3
C₂₂H₁₇NO₂⁽¹⁸⁾OS

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / 4 h / 20 °C / Inert atmosphere

2.1: tetrahydrofuran / 3 h / Reflux; Inert atmosphere

2.2: 0.17 h / 20 °C / Inert atmosphere; Saturated solution

3.1: N-iodo-succinimide; 2-(dicyclohexylphosphino)-2',4',6'-triisopropylbiphenyl Au bis(trifluoromethylsulfonyl)imide; ¹⁸O-labeled water / acetone / 16 h / Inert atmosphere; Reflux

With pyridine; N-iodo-succinimide; 2-(dicyclohexylphosphino)-2',4',6'-triisopropylbiphenyl Au bis(trifluoromethylsulfonyl)imide; ¹⁸O-labeled water; In tetrahydrofuran; acetone;
DOI:10.1021/jo201208e