Methanesulfonic acid (diethoxy-phosphoryl)-(4-methoxy-phenyl)-methyl ester

Base Information

Chemical Name:Methanesulfonic acid (diethoxy-phosphoryl)-(4-methoxy-phenyl)-methyl ester
CAS No.:99686-08-5
Molecular Formula:C₁₃H₂₁O₇PS
Molecular Weight:352.345
Hs Code.:

Synonyms:Methanesulfonic acid (diethoxy-phosphoryl)-(4-methoxy-phenyl)-methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanesulfonic acid (diethoxy-phosphoryl)-(4-methoxy-phenyl)-methyl ester

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Technology Process of Methanesulfonic acid (diethoxy-phosphoryl)-(4-methoxy-phenyl)-methyl ester

There total 3 articles about Methanesulfonic acid (diethoxy-phosphoryl)-(4-methoxy-phenyl)-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Diethyl phosphonate: 762-04-9,123-22-8
Diethyl phosphonate

: 123-11-5
4-methoxy-benzaldehyde

: 124-63-0
methanesulfonyl chloride

: 99686-08-5
Methanesulfonic acid (diethoxy-phosphoryl)-(4-methoxy-phenyl)-methyl ester

Guidance literature:: With triethylamine; Multistep reaction; 1.) 75 deg C, 30 min, 2.) CH₂Cl₂, RT, 2 h;
DOI:10.1055/s-1996-4242

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 99686-08-5
Methanesulfonic acid (diethoxy-phosphoryl)-(4-methoxy-phenyl)-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: KF; Al₂O₃

With aluminum oxide; potassium fluoride;
DOI:10.1080/10426500214892