C₃₃H₂₈NO₄⁽¹⁺⁾

Base Information

Chemical Name:C₃₃H₂₈NO₄⁽¹⁺⁾
CAS No.:1411713-95-5
Molecular Formula:C₃₃H₂₈NO₄
Molecular Weight:502.59
Hs Code.:

C<sub>33</sub>H<sub>28</sub>NO<sub>4</sub><sup>(1+)</sup>

Synonyms:C₃₃H₂₈NO₄⁽¹⁺⁾

Suppliers and Price of C₃₃H₂₈NO₄⁽¹⁺⁾

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₂₈NO₄⁽¹⁺⁾

Chemical Property:

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Technology Process of C₃₃H₂₈NO₄⁽¹⁺⁾

There total 9 articles about C₃₃H₂₈NO₄⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1411714-34-5
C₃₂H₂₉NO₄

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1411713-95-5
C₃₃H₂₈NO₄⁽¹⁺⁾

Guidance literature:: With trichlorophosphate; at 0 - 10 ℃; for 2.25h; Inert atmosphere;
DOI:10.1016/j.bmcl.2012.08.123

Reference yield:

: 72912-38-0
(2-bromo-3,4-dimethoxyphenyl)methanol

: 1411713-95-5
C₃₃H₂₈NO₄⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 9 steps

1: hydrogenchloride / toluene

2: dimethyl sulfoxide

3: sulfuric acid; water; acetic acid

4: oxalyl dichloride / dichloromethane / 2 h

5: sodium carbonate / chloroform / 0 °C / Inert atmosphere

6: bis-triphenylphosphine-palladium(II) chloride; caesium carbonate / 1,4-dioxane / 0.17 h / 120 °C / Microwave irradiation

7: trichlorophosphate / acetonitrile / 1 h / Reflux

8: tetralin; 10% Pd/C / Reflux; Inert atmosphere

9: trichlorophosphate / 2.25 h / 0 - 10 °C / Inert atmosphere

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; oxalyl dichloride; tetralin; sulfuric acid; 10% Pd/C; water; sodium carbonate; caesium carbonate; acetic acid; trichlorophosphate; In 1,4-dioxane; dichloromethane; chloroform; dimethyl sulfoxide; toluene; acetonitrile; 6: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2012.08.123

Reference yield:

: 7477-50-1
2-bromo-1-chloromethyl-3,4-dimethoxy-benzene

: 1411713-95-5
C₃₃H₂₈NO₄⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 8 steps

1: dimethyl sulfoxide

2: sulfuric acid; water; acetic acid

3: oxalyl dichloride / dichloromethane / 2 h

4: sodium carbonate / chloroform / 0 °C / Inert atmosphere

5: bis-triphenylphosphine-palladium(II) chloride; caesium carbonate / 1,4-dioxane / 0.17 h / 120 °C / Microwave irradiation

6: trichlorophosphate / acetonitrile / 1 h / Reflux

7: tetralin; 10% Pd/C / Reflux; Inert atmosphere

8: trichlorophosphate / 2.25 h / 0 - 10 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; oxalyl dichloride; tetralin; sulfuric acid; 10% Pd/C; water; sodium carbonate; caesium carbonate; acetic acid; trichlorophosphate; In 1,4-dioxane; dichloromethane; chloroform; dimethyl sulfoxide; acetonitrile; 5: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2012.08.123