meso-mono<α-o-<3,5-bis<(methyloxy)carbonyl>benzenecarboxamido>phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

Base Information

• Chemical Name: meso-mono<α-o-<3,5-bis<(methyloxy)carbonyl>benzenecarboxamido>phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin
• CAS No.: 139870-33-0
• Molecular Formula: C₇₀H₆₆N₈O₈
• Molecular Weight: 1147.34

Synonyms:meso-mono<α-o-<3,5-bis<(methyloxy)carbonyl>benzenecarboxamido>phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

Chemical Property of meso-mono<α-o-<3,5-bis<(methyloxy)carbonyl>benzenecarboxamido>phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

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Technology Process of meso-mono<α-o-<3,5-bis<(methyloxy)carbonyl>benzenecarboxamido>phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

There total 6 articles about meso-mono<α-o-<3,5-bis<(methyloxy)carbonyl>benzenecarboxamido>phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3,5-benzene tris(carbonyl chloride) (4422-95-1) → meso-mono<α-o-<3,5-bis<(methyloxy)carbonyl>benzenecarboxamido>phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin (139870-33-0)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂

2: pyridine / CH₂Cl₂

With pyridine; In dichloromethane;

Reference yield:

pivaloyl chloride (3282-30-2) → meso-mono<α-o-<3,5-bis<(methyloxy)carbonyl>benzenecarboxamido>phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin (139870-33-0)

Guidance literature:

Multi-step reaction with 4 steps

1: K₂CO₃ / CH₂Cl₂ / 3 h / 0 °C

2: Cl₃CCOOH / CH₂Cl₂ / 0 °C

3: pyridine / CH₂Cl₂

4: pyridine / CH₂Cl₂

With pyridine; potassium carbonate; trichloroacetic acid; In dichloromethane;

Reference yield:

meso-β-(o-aminophenyl)-α,α,α-tris<(o-pyvalamido)phenyl>porphyrin (75557-89-0) → meso-mono<α-o-<3,5-bis<(methyloxy)carbonyl>benzenecarboxamido>phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin (139870-33-0)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂

2: pyridine / CH₂Cl₂

With pyridine; In dichloromethane;

upstream raw materials:

methanol

1,3,5-benzene tris(carbonyl chloride)

pivaloyl chloride

meso-β-(o-aminophenyl)-α,α,α-tris<(o-pyvalamido)phenyl>porphyrin

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