[N-tert-butoxycarbonyl-N-(2-phenyldimethylsilylbut-2(Z)-enyl)amino]acetic acid

Base Information

Chemical Name:[N-tert-butoxycarbonyl-N-(2-phenyldimethylsilylbut-2(Z)-enyl)amino]acetic acid
CAS No.:320618-85-7
Molecular Formula:C₁₉H₂₉NO₄Si
Molecular Weight:363.529
Hs Code.:

Synonyms:[N-tert-butoxycarbonyl-N-(2-phenyldimethylsilylbut-2(Z)-enyl)amino]acetic acid

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Chemical Property of [N-tert-butoxycarbonyl-N-(2-phenyldimethylsilylbut-2(Z)-enyl)amino]acetic acid

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Technology Process of [N-tert-butoxycarbonyl-N-(2-phenyldimethylsilylbut-2(Z)-enyl)amino]acetic acid

There total 6 articles about [N-tert-butoxycarbonyl-N-(2-phenyldimethylsilylbut-2(Z)-enyl)amino]acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 320618-86-8
N-tert-butoxycarbonyl-N-[2-(dimethylphenylsilanyl)but-2(Z)-enyl]glycine methyl ester

: 320618-85-7
[N-tert-butoxycarbonyl-N-(2-phenyldimethylsilylbut-2(Z)-enyl)amino]acetic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 21h;
DOI:10.1039/b506198a

Reference yield: 63.0%

: 4530-20-5
BOC-glycine

: 320618-66-4
1-bromo-2-(dimethylphenylsilanyl)but-2(E)-ene

: 320618-85-7
[N-tert-butoxycarbonyl-N-(2-phenyldimethylsilylbut-2(Z)-enyl)amino]acetic acid

Guidance literature:: BOC-glycine; With potassium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

1-bromo-2-(dimethylphenylsilanyl)but-2(E)-ene; In N,N-dimethyl-formamide; at 20 ℃; for 14h; Further stages.;
DOI:10.1021/jo0056343

Reference yield:

: 31954-27-5
N-(tert-butoxycarbonyl)glycine methyl ester

: 320618-85-7
[N-tert-butoxycarbonyl-N-(2-phenyldimethylsilylbut-2(Z)-enyl)amino]acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / KH / tetrahydrofuran / 0 - 20 °C

2: 97 percent / aq. NaOH / tetrahydrofuran / 21 h / 20 °C

With sodium hydroxide; potassium hydride; In tetrahydrofuran;
DOI:10.1039/b506198a