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N-Ethylmethylamine
Cas No: 624-78-2
USD $ 1.0-1.0 / Milligram 1 Milligram 50000000 Kilogram/Year Xiamen Jenny Chemical Technology Co., Ltd. Contact Supplier
N-Ethylmethylamine Manufacturer/High quality/Best price/In stock
Cas No: 624-78-2
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
High purity Various Specifications ethyl(methyl)amine CAS:624-78-2
Cas No: 624-78-2
USD $ 100.0-500.0 / Gram 1 Gram 99999 Gram/Year Hangzhou Dingyan Chem Co., Ltd Contact Supplier
Factory Supply Ethyl(methyl)amine
Cas No: 624-78-2
No Data 1 1 Ality Chemical Corporation Contact Supplier
Amadis Chemical offer CAS#624-78-2;CAT#A8636
Cas No: 624-78-2
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
N-ETHYLMETHYLAMINE 624-78-2
Cas No: 624-78-2
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Manufacturer supply CAS 624-78-2 with competitive price
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USD $ 146.0-176.0 / Gram 10 Gram 1000 Kilogram/Day Zhuozhou Wenxi import and Export Co., Ltd Contact Supplier
BLOOM TECH Advanced API/Technology support N-EthylMethylaMine CAS 624-78-2
Cas No: 624-78-2
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whmulei API MSDS GMP COA china supplier cas 624-78-2 Ethylmethylamine china supplier
Cas No: 624-78-2
USD $ 6.0-12.0 / Gram 50 Gram 100000 Kilogram/Day WUHAN MULEI NEW MATERIAL CO., LTD Contact Supplier
CAS NO.:624-78-2
Cas No: 624-78-2
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624-78-2 Usage

Chemical Properties

clear colorless to light yellow liquid
InChI:InChI=1/C3H9N/c1-3-4-2/h4H,3H2,1-2H3

624-78-2 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (L04372)  N-Ethylmethylamine, 98+%    624-78-2 5g 432.0CNY Detail
Alfa Aesar (L04372)  N-Ethylmethylamine, 98+%    624-78-2 25g 1788.0CNY Detail

624-78-2SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name N-Ethylmethylamine

1.2 Other means of identification

Product number -
Other names 2-MAE

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:624-78-2 SDS

624-78-2Synthetic route

acetaldehyde
75-07-0

acetaldehyde

methylamine
74-89-5

methylamine

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

Conditions
ConditionsYield
With hydrogen; sodium hydroxide; Raney nickel at 65 - 67℃; under 22502.3 Torr; for 4.3h; Product distribution / selectivity; Autoclave; Industry scale;90%
With potassium hydroxide; dipotassium hydrogenphosphate; phosphoric acid at 10 - 12℃; for 4h; electrochemical reductive amination, lead cathode, current density 0.05 A/cm2, pH 12; Yield given;
With imine reductase from Streptomyces ipomoeae; NADPH In water at 30℃; for 0.166667h; pH=9.5; Catalytic behavior; Reagent/catalyst; Enzymatic reaction;
N-ethylidenemethylamine
6898-67-5

N-ethylidenemethylamine

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

Conditions
ConditionsYield
With hydrogen; platinum(IV) oxide In ethanol80%
N-ethyl-N-hydroxy-ethanamine
3710-84-7

N-ethyl-N-hydroxy-ethanamine

A

formaldehyd
50-00-0

formaldehyd

B

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

C

ethylamine
75-04-7

ethylamine

D

acetaldehyde
75-07-0

acetaldehyde

Conditions
ConditionsYield
With phosphorus pentachloride In toluene at 18 - 20℃; Mechanism; Product distribution; object of study: Stieglitz rearrangement (prototype);A n/a
B 1.4%
C 76%
D n/a
N-(benzylidene)ethylamine
6852-54-6

N-(benzylidene)ethylamine

(ethoxycarbonylmethyl)dimethylsulfonium bromide
5187-82-6

(ethoxycarbonylmethyl)dimethylsulfonium bromide

A

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

B

1-methylthio-3-phenyl-1,2-cyclopropanedicarboxylic acid diethyl ester
94117-87-0

1-methylthio-3-phenyl-1,2-cyclopropanedicarboxylic acid diethyl ester

Conditions
ConditionsYield
With potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride In tetrahydrofuran at 20℃; for 4h;A n/a
B 50%
pyridine
110-86-1

pyridine

N,N-diethylnmethylamine
616-39-7

N,N-diethylnmethylamine

dibenzoyl peroxide
94-36-0

dibenzoyl peroxide

A

formaldehyd
50-00-0

formaldehyd

B

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

C

acetaldehyde
75-07-0

acetaldehyde

D

diethylamine
109-89-7

diethylamine

diethyl ether
60-29-7

diethyl ether

N-chloromethylamine
6154-14-9

N-chloromethylamine

diethylzinc
557-20-0

diethylzinc

A

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

B

methylamine
74-89-5

methylamine

N,N-dichloromethylamine
7651-91-4

N,N-dichloromethylamine

diethylzinc
557-20-0

diethylzinc

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

Conditions
ConditionsYield
With Petroleum ether
N-nitrosomethylethylamine
10595-95-6

N-nitrosomethylethylamine

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

Conditions
ConditionsYield
With hydrogenchloride
N-ethyl-N-methylbenzylamine
4788-37-8

N-ethyl-N-methylbenzylamine

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

Conditions
ConditionsYield
With platinum(IV) oxide; acetic acid at 65 - 75℃; under 2206.5 Torr; durch Hydrogenolyse;
ethylamine
75-04-7

ethylamine

methyl iodide
74-88-4

methyl iodide

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

Conditions
ConditionsYield
With ethanol at 100℃;
1-Ethyl-1-methylpyrrolidinium iodide
4186-68-9

1-Ethyl-1-methylpyrrolidinium iodide

ethanolamine
141-43-5

ethanolamine

A

1-Methylpyrrolidine
120-94-5

1-Methylpyrrolidine

B

1-ethylpyrrolidine
7335-06-0

1-ethylpyrrolidine

C

1-pyrrolidineethanol
2955-88-6

1-pyrrolidineethanol

D

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

ethyl isocyanate
109-90-0

ethyl isocyanate

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

Conditions
ConditionsYield
With lithium aluminium tetrahydride; 3,6,9-trioxaundecane
With hydrogen; nickel at 180 - 190℃;
acetic anhydride
108-24-7

acetic anhydride

A

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

B

3.7.3'.7'-Tetramethoxy-4.6.4'.6'-tetraacetoxy-diphenanthryl-(1.1')

3.7.3'.7'-Tetramethoxy-4.6.4'.6'-tetraacetoxy-diphenanthryl-(1.1')

Conditions
ConditionsYield
at 180℃; isomer(ic) I;
MORPHIN
57-27-2

MORPHIN

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

Conditions
ConditionsYield
With potassium hydroxide at 180℃;
N-Diphenylmethylen(ethyl)amin
27126-11-0

N-Diphenylmethylen(ethyl)amin

methyl iodide
74-88-4

methyl iodide

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

Conditions
ConditionsYield
Kochen des endstandenen Jodmethylats mit Alkohol;
methyl bromide
74-83-9

methyl bromide

diethyl N-ethylphosphoramidate
1946-09-4

diethyl N-ethylphosphoramidate

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

Conditions
ConditionsYield
(i) aq. NaOH, HSO4, (ii) HCl; Multistep reaction;
N-(benzylidene)ethylamine
6852-54-6

N-(benzylidene)ethylamine

dimethyl sulfate
77-78-1

dimethyl sulfate

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

ethyl bromide
74-96-4

ethyl bromide

methylamine
74-89-5

methylamine

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

Conditions
ConditionsYield
In ethanol at 100℃; under 3677.5 Torr;
1,3,5-triethyl-1,3,5-triazacyclohexane
7779-27-3

1,3,5-triethyl-1,3,5-triazacyclohexane

mono-trimethylsilylphosphite
91076-68-5

mono-trimethylsilylphosphite

A

N,N-dimethyl-ethanamine
598-56-1

N,N-dimethyl-ethanamine

B

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

N-Ethyl,N-methylacetamide
38806-26-7

N-Ethyl,N-methylacetamide

A

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

B

acetate
71-50-1

acetate

Conditions
ConditionsYield
With sodium hydroxide In water at 100℃; Rate constant; Mechanism;
triphenylmethane
519-73-3

triphenylmethane

lithium ethylmethyl amide
57018-31-2

lithium ethylmethyl amide

A

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

B

trityllithium
733-90-4

trityllithium

Conditions
ConditionsYield
In tetrahydrofuran at 30℃; Equilibrium constant;
N-Methyl-N-ethylamino-triphenyl-phosphonium-jodid

N-Methyl-N-ethylamino-triphenyl-phosphonium-jodid

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

Conditions
ConditionsYield
With water; hydroxide
nitrogen mustard
51-75-2

nitrogen mustard

A

ethanol
64-17-5

ethanol

B

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

C

N,N-diethylnmethylamine
616-39-7

N,N-diethylnmethylamine

Conditions
ConditionsYield
With potassium hydroxide; aluminum nickel In methanol Product distribution; degradation under various conditions with preparation of nonmutagenic reaction mixtures of products;
propiononitrile
107-12-0

propiononitrile

Devarda's's alloy

Devarda's's alloy

A

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

B

methyl-n-propylamine
627-35-0

methyl-n-propylamine

C

ethylamine
75-04-7

ethylamine

D

propionaldehyde
123-38-6

propionaldehyde

Conditions
ConditionsYield
weiteres Produkt:Ammoniak;
propiononitrile
107-12-0

propiononitrile

magnesium copper

magnesium copper

A

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

B

methyl-n-propylamine
627-35-0

methyl-n-propylamine

C

ethylamine
75-04-7

ethylamine

D

propionaldehyde
123-38-6

propionaldehyde

Conditions
ConditionsYield
weiteres Produkt:Ammoniak;
ethyl isocyanate
109-90-0

ethyl isocyanate

hydrogen

hydrogen

nickel

nickel

A

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

B

ammonia
7664-41-7

ammonia

C

ethylamine
75-04-7

ethylamine

D

diethylamine
109-89-7

diethylamine

Conditions
ConditionsYield
at 180 - 190℃; Produkt 5: Triaethylamin;
1.3.5-triethyl-hexahydro-1.3.5-triazine

1.3.5-triethyl-hexahydro-1.3.5-triazine

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

Conditions
ConditionsYield
With hydrogenchloride; zinc zuletzt bei Siedetemperatur;
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

indole-2,3-dione
91-56-5

indole-2,3-dione

(2-Amino-phenyl)-oxo-acetic acid; compound with ethyl-methyl-amine

(2-Amino-phenyl)-oxo-acetic acid; compound with ethyl-methyl-amine

Conditions
ConditionsYield
In water Heating;100%
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

4-[phenyl(endo-8-methyl-8-azabicyclo[3.2.1]octan-3-yl)amino]benzoic acid
287721-05-5

4-[phenyl(endo-8-methyl-8-azabicyclo[3.2.1]octan-3-yl)amino]benzoic acid

N-ethyl-N-methyl-4-[(8-methyl-8-aza-bicyclo[3.2.1]oct-3-yl)-phenyl-amino]-benzamide
287720-97-2

N-ethyl-N-methyl-4-[(8-methyl-8-aza-bicyclo[3.2.1]oct-3-yl)-phenyl-amino]-benzamide

Conditions
ConditionsYield
With N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate Acylation;100%
C16H20N2O5S

C16H20N2O5S

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

ethyl-methyl-{3-[3-(4-methyl-piperidin-1-yl)-4-nitro-phenyl]-prop-2-ynyl}-amine
954424-88-5

ethyl-methyl-{3-[3-(4-methyl-piperidin-1-yl)-4-nitro-phenyl]-prop-2-ynyl}-amine

Conditions
ConditionsYield
In dichloromethane for 0.333333h; Heating / reflux;100%
3-[3-(phenylsulfonyl)-1H-indol-4-yl]propyl 4-methylbenzenesulfonate
945001-04-7

3-[3-(phenylsulfonyl)-1H-indol-4-yl]propyl 4-methylbenzenesulfonate

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

N-ethyl-N-methyl-3-[3-(phenylsulfonyl)-1H-indol-4-yl]propan-1-amine hydrochloride

N-ethyl-N-methyl-3-[3-(phenylsulfonyl)-1H-indol-4-yl]propan-1-amine hydrochloride

Conditions
ConditionsYield
Stage #1: 3-[3-(phenylsulfonyl)-1H-indol-4-yl]propyl 4-methylbenzenesulfonate; N-Ethylmethylamine In tetrahydrofuran at 65℃; for 16h;
Stage #2: With sodium hydroxide; water In tetrahydrofuran
100%
Stage #1: 3-[3-(phenylsulfonyl)-1H-indol-4-yl]propyl 4-methylbenzenesulfonate; N-Ethylmethylamine In tetrahydrofuran at 65℃; for 16h;
Stage #2: With hydrogenchloride In ethanol
69%
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

2,4-dichloro-8-phenyl-7,8-dihydro-5H-pyrano[4,3-d]pyrimidine
1263868-77-4

2,4-dichloro-8-phenyl-7,8-dihydro-5H-pyrano[4,3-d]pyrimidine

2-chloro-N-ethyl-N-methyl-8-phenyl-7,8-dihydro-5H-pyrano[4,3-d]pyrimidin-4-amine
1263868-83-2

2-chloro-N-ethyl-N-methyl-8-phenyl-7,8-dihydro-5H-pyrano[4,3-d]pyrimidin-4-amine

Conditions
ConditionsYield
In methanol at 20℃; for 1h;100%
In methanol at 20℃; for 1h;100%
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

2,4-dichloro-8-(4-fluorophenyl)-5,6,7,8-tetrahydroquinazoline
1263870-09-2

2,4-dichloro-8-(4-fluorophenyl)-5,6,7,8-tetrahydroquinazoline

2-chloro-N-ethyl-8-(4-fluorophenyl)-N-methyl-5,6,7,8-tetrahydroquinazolin-4-amine
1263870-13-8

2-chloro-N-ethyl-8-(4-fluorophenyl)-N-methyl-5,6,7,8-tetrahydroquinazolin-4-amine

Conditions
ConditionsYield
In methanol at 20℃; for 0.5h;100%
In methanol at 20℃; for 0.5h;100%
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

2,4-dichloro-7-phenyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine
1263868-24-1

2,4-dichloro-7-phenyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine

2-chloro-N-ethyl-N-methyl-7-phenyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-4-amine
1263868-27-4

2-chloro-N-ethyl-N-methyl-7-phenyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-4-amine

Conditions
ConditionsYield
In methanol at 20℃; for 1h;100%
In methanol at 20℃; for 1h;100%
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

3-methoxy-4-methyl-3-cyclobutene-1,2-dione
29769-77-5

3-methoxy-4-methyl-3-cyclobutene-1,2-dione

3-(ethyl(methyl)amino)-4-methylcyclobut-3-ene-1,2-dione

3-(ethyl(methyl)amino)-4-methylcyclobut-3-ene-1,2-dione

Conditions
ConditionsYield
In methanol at 20℃; for 4h;100%
carbon disulfide
75-15-0

carbon disulfide

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

lithium N-ethyl-N-methyldithiocarbamate

lithium N-ethyl-N-methyldithiocarbamate

Conditions
ConditionsYield
Stage #1: N-Ethylmethylamine With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.25h;
Stage #2: carbon disulfide In tetrahydrofuran; hexane at 20℃; for 3h;
100%
N-(tert-butyloxycarbonyl)-L-isoleucine
13139-16-7

N-(tert-butyloxycarbonyl)-L-isoleucine

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

N-[N-(tert-butyloxycarbonyl)-L-isoleucyl]-N-ethyl-N-methylamine

N-[N-(tert-butyloxycarbonyl)-L-isoleucyl]-N-ethyl-N-methylamine

Conditions
ConditionsYield
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate In triethylamine; N,N-dimethyl-formamide Ambient temperature;99%
4-(2-ethyl-3-chloropyridyl-4-oxy)-2,5-xylidine

4-(2-ethyl-3-chloropyridyl-4-oxy)-2,5-xylidine

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

trimethyl orthoformate
149-73-5

trimethyl orthoformate

N-ethyl-N-methyl-N'-[4-(2-ethyl-3-chloropyridyl-4-oxy)-2,5-xylyl]formamidine

N-ethyl-N-methyl-N'-[4-(2-ethyl-3-chloropyridyl-4-oxy)-2,5-xylyl]formamidine

Conditions
ConditionsYield
Stage #1: 4-(2-ethyl-3-chloropyridyl-4-oxy)-2,5-xylidine; trimethyl orthoformate With toluene-4-sulfonic acid for 3h; Heating / reflux;
Stage #2: N-Ethylmethylamine In dichloromethane at 20℃; for 16h;
99%
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

methyl 2-(methylthio)benzo[d]oxazole-6-carboxylate
1160490-11-8

methyl 2-(methylthio)benzo[d]oxazole-6-carboxylate

C12H14N2O3
1160490-12-9

C12H14N2O3

Conditions
ConditionsYield
In tetrahydrofuran at 70℃;99%
In tetrahydrofuran at 70℃;
carbon disulfide
75-15-0

carbon disulfide

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

C2H5CH3NC(S)SSC(S)NCH3C2H5
155722-99-9

C2H5CH3NC(S)SSC(S)NCH3C2H5

Conditions
ConditionsYield
With oxygen In isopropyl alcohol at 50℃; under 1275.13 Torr; for 2h; Autoclave;98.6%
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

N,N-chloromethylethylamine
36260-79-4

N,N-chloromethylethylamine

Conditions
ConditionsYield
With N-chloro-succinimide under 0.004 Torr; Ambient temperature; stored at t<-20 deg C;98%
With N-chloro-succinimide under 1E-05 Torr; Ambient temperature; Yield given;
With sodium hypochlorite; sodium perchlorate In water at 24.85℃; Kinetics; Further Variations:; Temperatures; Chlorination;
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

m-anisoyl chloride
1711-05-3

m-anisoyl chloride

N-ethyl-3-methoxy-N-methylbenzamide
207558-42-7

N-ethyl-3-methoxy-N-methylbenzamide

Conditions
ConditionsYield
In dichloromethane at 0℃; for 2h;98%
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

1-(6-bromo-3,4-dihydroquinolin-1(2H)-yl)-2-chloroethanone
942035-74-7

1-(6-bromo-3,4-dihydroquinolin-1(2H)-yl)-2-chloroethanone

1-(6-bromo-3,4-dihydroquinolin-1(2H)-yl)-2-(ethyl(methyl)amino)ethanone
1063408-94-5

1-(6-bromo-3,4-dihydroquinolin-1(2H)-yl)-2-(ethyl(methyl)amino)ethanone

Conditions
ConditionsYield
With potassium iodide In tetrahydrofuran at 20 - 65℃; for 3h;98%
With potassium iodide In tetrahydrofuran at 20 - 65℃; for 3h; Inert atmosphere;98%
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

triisopropylchlorogermane
2816-54-8

triisopropylchlorogermane

ethylmethylaminotriisopropylgermane
1147551-48-1

ethylmethylaminotriisopropylgermane

Conditions
ConditionsYield
Stage #1: N-Ethylmethylamine With n-butyllithium In diethyl ether at 0℃; for 2h; Cooling with ice;
Stage #2: triisopropylchlorogermane In diethyl ether at 0 - 20℃;
98%
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

6-Chloropurine riboside
2004-06-0

6-Chloropurine riboside

(2R,3R,4S,5R)-2-(6-(ethyl(methyl)amino)-9H-purin-9-yl)-5-(hydroxymethyl)tetrahydrofuran-3,4-diol

(2R,3R,4S,5R)-2-(6-(ethyl(methyl)amino)-9H-purin-9-yl)-5-(hydroxymethyl)tetrahydrofuran-3,4-diol

Conditions
ConditionsYield
With triethylamine In ethanol at 60℃; for 18h;98%
With triethylamine In ethanol Reflux;0.93 g
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

4-isocyanobenzenesulfonyl chloride

4-isocyanobenzenesulfonyl chloride

N-ethyl-4-isocyano-N-methylbenzenesulfonamide

N-ethyl-4-isocyano-N-methylbenzenesulfonamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 25℃; for 1h;98%
N-hydroxyphthalimide
524-38-9

N-hydroxyphthalimide

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

N-ethyl-2-(3-ethyl-3-methylureido)-N-methylbenzamide

N-ethyl-2-(3-ethyl-3-methylureido)-N-methylbenzamide

Conditions
ConditionsYield
With triethyl phosphite In toluene at 50℃; for 12h;98%
3-(1-hydroxy-1-phenyl-methylene)-6-carboxy-2-indolinone

3-(1-hydroxy-1-phenyl-methylene)-6-carboxy-2-indolinone

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

3-(1-hydroxy-1-phenyl-methylene)-6-(N-ethyl-methylcarbamoyl)-2-indolinone

3-(1-hydroxy-1-phenyl-methylene)-6-(N-ethyl-methylcarbamoyl)-2-indolinone

Conditions
ConditionsYield
With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 12h;97%
2-[3-(phenylsulfonyl)-1H-indol-4-yl]ethyl 4-methylbenzenesulfonate
945000-91-9

2-[3-(phenylsulfonyl)-1H-indol-4-yl]ethyl 4-methylbenzenesulfonate

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

N-ethyl-N-methyl-N-{2-[3-(phenylsulfonyl)-1H-indol-4-yl]ethyl}amine hydrochloride

N-ethyl-N-methyl-N-{2-[3-(phenylsulfonyl)-1H-indol-4-yl]ethyl}amine hydrochloride

Conditions
ConditionsYield
Stage #1: 2-[3-(phenylsulfonyl)-1H-indol-4-yl]ethyl 4-methylbenzenesulfonate; N-Ethylmethylamine In tetrahydrofuran at 71℃; for 24h;
Stage #2: With ammonia In ethanol; dichloromethane
Stage #3: With hydrogenchloride; water In diethyl ether
97%
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

(Z)-3-(hydroxy-phenyl-methylene)-2-oxo-2,3-dihydro-1H-indole-6-carboxylic acid
1253768-91-0

(Z)-3-(hydroxy-phenyl-methylene)-2-oxo-2,3-dihydro-1H-indole-6-carboxylic acid

(Z)-3-(hydroxy-phenyl-methylene)-2-oxo-2,3-dihydro-1H-indole-6-carboxylic acid N-methyl-N-ethylamide
1253768-93-2

(Z)-3-(hydroxy-phenyl-methylene)-2-oxo-2,3-dihydro-1H-indole-6-carboxylic acid N-methyl-N-ethylamide

Conditions
ConditionsYield
Stage #1: (Z)-3-(hydroxy-phenyl-methylene)-2-oxo-2,3-dihydro-1H-indole-6-carboxylic acid With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 0.5h;
Stage #2: N-Ethylmethylamine In N,N-dimethyl-formamide at 20℃; for 24h;
97%
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

ethyl 2-chloro-5-methyloxazole-4-carboxylate
1144520-57-9

ethyl 2-chloro-5-methyloxazole-4-carboxylate

ethyl 2-(N-ethylmethylamino)-5-methyloxazole-4-carboxylate

ethyl 2-(N-ethylmethylamino)-5-methyloxazole-4-carboxylate

Conditions
ConditionsYield
at 20℃; for 13.5h;97%
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

ethyl 8-bromo-2-chloroimidazo[1,2-b]pyridazine-7-carboxylate

ethyl 8-bromo-2-chloroimidazo[1,2-b]pyridazine-7-carboxylate

ethyl 2-chloro-8-(ethyl(methyl)amino)imidazo[1,2-b]pyridazine-7-carboxylate

ethyl 2-chloro-8-(ethyl(methyl)amino)imidazo[1,2-b]pyridazine-7-carboxylate

Conditions
ConditionsYield
In tetrahydrofuran at 0 - 20℃; Inert atmosphere;96.7%
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

(R,E)-2-((4-(3,5-dimethoxystyryl)phenoxy)methyl)oxirane

(R,E)-2-((4-(3,5-dimethoxystyryl)phenoxy)methyl)oxirane

(R,E)-1-(4-(3,5-dimethoxystyryl)phenoxy)-3-(ethyl(methyl)amino)propan-2-ol

(R,E)-1-(4-(3,5-dimethoxystyryl)phenoxy)-3-(ethyl(methyl)amino)propan-2-ol

Conditions
ConditionsYield
In methanol at 65℃; Inert atmosphere; Darkness;96.3%
[2-(3-isopropyl-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl)-benzyl]-carbamic acid phenyl ester

[2-(3-isopropyl-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl)-benzyl]-carbamic acid phenyl ester

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

1-ethyl-3-[2-(3-isopropyl-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl)-benzyl]-1-methyl-urea
745827-35-4

1-ethyl-3-[2-(3-isopropyl-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl)-benzyl]-1-methyl-urea

Conditions
ConditionsYield
Stage #1: [2-(3-isopropyl-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl)-benzyl]-carbamic acid phenyl ester; N-Ethylmethylamine In dimethyl sulfoxide at 20℃; for 0.5h;
Stage #2: In water
96%
methyl 5-chloro-7-[(3-methylphenyl)amino]-1-[2-(2,2,2-trifluoroethoxy)ethyl]-1H-pyrazolo[4,3-d]pyrimidine-3-carboxylate

methyl 5-chloro-7-[(3-methylphenyl)amino]-1-[2-(2,2,2-trifluoroethoxy)ethyl]-1H-pyrazolo[4,3-d]pyrimidine-3-carboxylate

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

C21H25F3N6O3

C21H25F3N6O3

Conditions
ConditionsYield
With cesium fluoride In dimethyl sulfoxide at 120℃; for 12h;96%
N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

phenylacetylene
536-74-3

phenylacetylene

C11H15N

C11H15N

Conditions
ConditionsYield
With C18H17N3Ni In toluene at 75℃; for 6h;96%
With C17H15N3Pd In toluene at 75℃; for 6h;93%
6-(methoxycarbonyl)pyridine-2-carboxylic acid
7170-36-7

6-(methoxycarbonyl)pyridine-2-carboxylic acid

N-Ethylmethylamine
624-78-2

N-Ethylmethylamine

6-(ethyl(methyl)carbamoyl)picolinic acid methyl ester

6-(ethyl(methyl)carbamoyl)picolinic acid methyl ester

Conditions
ConditionsYield
With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 5h;96%
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