N-(2,2,2-trichloro-1,1-dimethyl-1-ethyloxycarbonyl)imidazolium tosylate

Base Information

Chemical Name:N-(2,2,2-trichloro-1,1-dimethyl-1-ethyloxycarbonyl)imidazolium tosylate
CAS No.:1374003-80-1
Molecular Formula:C₇H₈O₃S*C₈H₉Cl₃N₂O₂
Molecular Weight:443.735
Hs Code.:

Synonyms:N-(2,2,2-trichloro-1,1-dimethyl-1-ethyloxycarbonyl)imidazolium tosylate

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Chemical Property of N-(2,2,2-trichloro-1,1-dimethyl-1-ethyloxycarbonyl)imidazolium tosylate

Chemical Property:

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Technology Process of N-(2,2,2-trichloro-1,1-dimethyl-1-ethyloxycarbonyl)imidazolium tosylate

There total 1 articles about N-(2,2,2-trichloro-1,1-dimethyl-1-ethyloxycarbonyl)imidazolium tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1346641-42-6
3,3,3-trichloro-2-methyl-2-propyl imidazole-1-carboxylate

: 104-15-4
toluene-4-sulfonic acid

: 1374003-80-1
N-(2,2,2-trichloro-1,1-dimethyl-1-ethyloxycarbonyl)imidazolium tosylate

Guidance literature:: In acetone; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tet.2012.02.044

Reference yield:

: 622-33-3
N-benzyloxyamine

: 1374003-80-1
N-(2,2,2-trichloro-1,1-dimethyl-1-ethyloxycarbonyl)imidazolium tosylate

: C₁₂H₁₄Cl₃NO₃

Guidance literature:: With 1H-imidazole; In acetonitrile; at 60 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2012.02.044

Reference yield:

: 1374003-80-1
N-(2,2,2-trichloro-1,1-dimethyl-1-ethyloxycarbonyl)imidazolium tosylate

: 1374003-05-0
1,1,1-trichloro-2-methylpropan-2-yl (tosyloxy)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / acetonitrile / 2 h / 60 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / methanol / 16 h

3: triethylamine / diethyl ether / 2 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; palladium 10% on activated carbon; hydrogen; triethylamine; In methanol; diethyl ether; acetonitrile;
DOI:10.1016/j.tet.2012.02.044