C₁₆H₁₂Cl₅F₃N₄OS

Base Information

Chemical Name:C₁₆H₁₂Cl₅F₃N₄OS
CAS No.:1222566-15-5
Molecular Formula:C₁₆H₁₂Cl₅F₃N₄OS
Molecular Weight:542.624
Hs Code.:

C<sub>16</sub>H<sub>12</sub>Cl<sub>5</sub>F<sub>3</sub>N<sub>4</sub>OS

Synonyms:C₁₆H₁₂Cl₅F₃N₄OS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₂Cl₅F₃N₄OS

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Technology Process of C₁₆H₁₂Cl₅F₃N₄OS

There total 5 articles about C₁₆H₁₂Cl₅F₃N₄OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 67-56-1
methanol

: 1222566-09-7
5-(2,2,2-trichloroethylideneamino)-3-cyano-1-(2,6-dichloro-4-trifluoromethylphenyl)-4-ethylsulfenylpyrazole

: 1222566-15-5
C₁₆H₁₂Cl₅F₃N₄OS

Guidance literature:: for 2h; Reflux;
DOI:10.1021/jf1001793

Reference yield:

: 24279-39-8
2,6-dichloro-4-(trifluoromethyl)aniline

: 1222566-15-5
C₁₆H₁₂Cl₅F₃N₄OS

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid; sodium nitrite / acetic acid / 0.67 h / 55 - 60 °C

1.2: 5 - 20 °C

1.3: 20 °C

2.1: disulfur dichloride / dichloromethane / 20 °C

3.1: dipotassium hydrogenphosphate; sodium dithionite / water; N,N-dimethyl-formamide / 4 h / 20 °C

4.1: 36 h / Reflux; Molecular sieve

5.1: 2 h / Reflux

With disulfur dichloride; dipotassium hydrogenphosphate; sodium dithionite; sulfuric acid; sodium nitrite; In dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jf1001793

Reference yield:

: 130755-46-3
4,4'-dithiobis [5-amino-3-cyano-1-{2,6-dichloro-4-(trifluoromethyl)phenyl}-1H-pyrazole]

: 1222566-15-5
C₁₆H₁₂Cl₅F₃N₄OS

Guidance literature:: Multi-step reaction with 3 steps

1: dipotassium hydrogenphosphate; sodium dithionite / water; N,N-dimethyl-formamide / 4 h / 20 °C

2: 36 h / Reflux; Molecular sieve

3: 2 h / Reflux

With dipotassium hydrogenphosphate; sodium dithionite; In water; N,N-dimethyl-formamide;
DOI:10.1021/jf1001793