Boc-γ-OBn

Base Information

Chemical Name:Boc-γ-OBn
CAS No.:1292321-01-7
Molecular Formula:C₂₂H₃₃NO₄
Molecular Weight:375.508
Hs Code.:

Synonyms:Boc-γ-OBn

Suppliers and Price of Boc-γ-OBn

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Boc-γ-OBn

Chemical Property:

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Technology Process of Boc-γ-OBn

There total 6 articles about Boc-γ-OBn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1194837-08-5
(S)-2-((1S,2S)-2-(tert-butoxycarbonylamino)cyclohexyl)butanoic acid

: 100-39-0
benzyl bromide

: 1292321-01-7
Boc-γ-OBn

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide;

Reference yield:

: 2562-37-0
1-nitrocyclohexene

: 1292321-01-7
Boc-γ-OBn

Guidance literature:: Multi-step reaction with 6 steps

1.1: 3-nitrobenzoic acid; (R)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine / dichloromethane / 0.02 h / 20 °C

1.2: 36 h / 23 °C

2.1: sodium tetrahydroborate; methanol / 0 °C

3.1: Jones reagent / acetone / 5 h / 0 - 20 °C

4.1: hydrogen / Raney nickel / methanol / 24 h / 2068.65 Torr / Inert atmosphere

5.1: chloro-trimethyl-silane / dichloromethane / 2 h / 20 °C

5.2: 12 h / 0 - 20 °C

6.1: caesium carbonate / N,N-dimethyl-formamide

With methanol; sodium tetrahydroborate; Jones reagent; chloro-trimethyl-silane; hydrogen; caesium carbonate; (R)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine; 3-nitrobenzoic acid; In methanol; dichloromethane; N,N-dimethyl-formamide; acetone; 1.1: Michael Condensation / 1.2: Michael Condensation;

Reference yield:

: 1194837-07-4
(S)-2-((1S,2S)-2-nitrocyclohexyl)butanoic acid:

: 1292321-01-7
Boc-γ-OBn

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / Raney nickel / methanol / 24 h / 2068.65 Torr / Inert atmosphere

2.1: chloro-trimethyl-silane / dichloromethane / 2 h / 20 °C

2.2: 12 h / 0 - 20 °C

3.1: caesium carbonate / N,N-dimethyl-formamide

With chloro-trimethyl-silane; hydrogen; caesium carbonate; Raney nickel; In methanol; dichloromethane; N,N-dimethyl-formamide;