2,3-bis(tert-butyldimethylsilyl ether)benzaldehyde

Base Information

Chemical Name:2,3-bis(tert-butyldimethylsilyl ether)benzaldehyde
CAS No.:757995-80-5
Molecular Formula:C₁₉H₃₄O₃Si₂
Molecular Weight:366.648
Hs Code.:

Synonyms:2,3-bis(tert-butyldimethylsilyl ether)benzaldehyde

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Chemical Property of 2,3-bis(tert-butyldimethylsilyl ether)benzaldehyde

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Technology Process of 2,3-bis(tert-butyldimethylsilyl ether)benzaldehyde

There total 1 articles about 2,3-bis(tert-butyldimethylsilyl ether)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 24677-78-9
2,3-dihydroxybenzaldehyde

: 18162-48-6
tert-butyldimethylsilyl chloride

: 757995-80-5
2,3-bis(tert-butyldimethylsilyl ether)benzaldehyde

Guidance literature:: With 1H-imidazole; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/acs.jmedchem.0c00388

Reference yield: 78.0%

: 757995-80-5
2,3-bis(tert-butyldimethylsilyl ether)benzaldehyde

: 3-((tert-butyldimethylsilyl)oxy)-2-hydroxybenzaldehyde

Guidance literature:: With zinc(II) chloride; In 1,2-dichloro-ethane; at 80 ℃;
DOI:10.1016/j.tetlet.2012.07.103

Reference yield: 76.0%

: 757995-80-5
2,3-bis(tert-butyldimethylsilyl ether)benzaldehyde

: 623-33-6
glycine ethyl ester hydrochloride

: ethyl (2,3-bis((tert-butyldimethylsilyl)oxy)benzyl)glycinate

Guidance literature:: 2,3-bis(tert-butyldimethylsilyl ether)benzaldehyde; glycine ethyl ester hydrochloride; With triethylamine; In 1,2-dichloro-ethane; at 20 ℃; for 6h; Molecular sieve;

With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 10 ℃; Inert atmosphere; Molecular sieve;
DOI:10.1021/acs.jmedchem.0c00388