Acetic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester

Base Information

• Chemical Name: Acetic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester
• CAS No.: 1027200-39-0
• Molecular Formula: C₃₄H₅₁NO₄
• Molecular Weight: 537.783

Synonyms:Acetic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester

Chemical Property of Acetic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester

Chemical Property:

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Technology Process of Acetic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester

There total 7 articles about Acetic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(4-hydroxyphenyl)propionic acid methyl ester (5597-50-2) → Acetic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester (1027200-39-0)

Guidance literature:

Multi-step reaction with 6 steps

1: potassium carbonate / acetone / Heating

2: aq. KOH / methanol

3: oxalyl chloride, DMF / CH₂Cl₂

4: pyridine / tetrahydrofuran / Ambient temperature

5: LiAlH₄ / tetrahydrofuran

6: pyridine / CH₂Cl₂

With pyridine; potassium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; dichloromethane; acetone;

DOI:10.1021/jm00104a002

Reference yield:

1-Bromotetradecane (112-71-0) → Acetic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester (1027200-39-0)

Guidance literature:

Multi-step reaction with 6 steps

1: potassium carbonate / acetone / Heating

2: aq. KOH / methanol

3: oxalyl chloride, DMF / CH₂Cl₂

4: pyridine / tetrahydrofuran / Ambient temperature

5: LiAlH₄ / tetrahydrofuran

6: pyridine / CH₂Cl₂

With pyridine; potassium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; dichloromethane; acetone;

DOI:10.1021/jm00104a002

Reference yield:

3-(4-Tetradecyloxy-phenyl)-propionic acid methyl ester (62442-94-8) → Acetic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester (1027200-39-0)

Guidance literature:

Multi-step reaction with 5 steps

1: aq. KOH / methanol

2: oxalyl chloride, DMF / CH₂Cl₂

3: pyridine / tetrahydrofuran / Ambient temperature

4: LiAlH₄ / tetrahydrofuran

5: pyridine / CH₂Cl₂

With pyridine; potassium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; dichloromethane;

DOI:10.1021/jm00104a002

upstream raw materials:

{3-[3-(4-Tetradecyloxy-phenyl)-propylamino]-phenyl}-methanol

acetyl chloride

1-Bromotetradecane

3-(4-Tetradecyloxy-phenyl)-propionic acid methyl ester

Downstream raw materials:

Methanesulfonic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester

N-(3-Hydroxymethyl-phenyl)-N-[3-(4-tetradecyloxy-phenyl)-propyl]-acetamide

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